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- MIR <br /> - <br /> y k iR 'S �ts•`C � mb Ie �? <br /> ggyy , n <br /> $YEk".�^ 2_". "°..tea. -a .4.afi`t'�i,• ��'.�`�i�y'�� - - .b '�sc <br /> t` • y• <br /> 1 <br /> K. Ice the sample vials immediately and keep them iced <br /> j through shipment. <br /> L. Fill out chain-of-custody form. SOP it gives major <br /> -- -- .details♦ Make sure sample requests is for proper _ <br /> analysis type. <br /> M. ` Shipping of hazardous materials (methanol) requires <br /> special documents from Federal Express and UPS. <br /> Briefly you will need to add following to outside of <br /> package and on documents: <br /> 1. Flammable liquid label (some will come from lab <br /> with the vials) . <br /> 2. "UN1230 methyl alcohol". <br /> 3. For UPS, a "Hazardous Material" Zabel. <br /> N. Ship overnight delivery to the lab. if dry ice is <br /> available, up to 5 pounds per package can be sent via <br /> Federal Express by simply writing "0P-74-A dry ice, <br /> pounds, for research" on outside of package and or, r <br /> shipping document. UPS does not accept dry-ice <br /> shipments. <br /> 5. Good sampling practice would include preparing one out of <br /> five samples to be prepared in duplicates for analysis. <br /> These four out of twenty samples will be for the following <br /> purposes: <br /> A. One in every twenty samples should be analyzed as a <br /> i field replicate to evaluate the precision of the <br /> sampling technique. A minimum of one sample per <br /> data set is suggested. <br /> B. An additional one in twenty samples should be selected <br /> } f by sampler to be prepared in duplicate as alternative <br /> to Step (A) . Choose a different ,soil type if <br /> available. <br /> C. The lab does spiking with reference materials for <br /> internal Quality Control (QC) so additionally a minimum <br /> of tuo in twenty samples need to be prepared in <br /> duplicate. <br /> i <br /> GkoINDUOIx <br /> NOW= M <br /> �k;l'fl\u�lk�1'.I�l <br />