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4 <br /> Lancaster <br /> . Analysis nalys�s Reporf <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605-2425•717-656 2300 Paz 717-656.2681•www lancasterlabs corn <br /> Page 4 of 4 <br /> Quality Control Summary <br /> C1-zent=Name =GhevronTexaco Group—Number- _879333 <br /> Reported 12/30/03 at 04 27 Pf+'I <br /> Surrogate Quality Control <br /> Batch number P033611AA <br /> Dibromofluoromethane 1,2-Dachloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4189768 98 96 103 96 <br /> 4189770 99 95 103 95 <br /> 4189771 100 98 103 97 <br /> 4189772 98 97 103 95 <br /> 4189773 99 97 103 96 <br /> 4169774 98 97 102 95 <br /> 4189775 99 97 102 95 <br /> Blank 99 97 103 95 <br /> LCS 100 97 103 96 <br /> MS 98 96 103 96 <br /> MSD 99 97 104 97 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB <br /> Batch number P033631AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4189767 99 98 103 96 <br /> 4189769 99 96 102 95 <br /> Blank 99 98 102 96 <br /> LCS 99 95 102 95 <br /> MS 100 97 103 96 <br /> MSD 99 97 102 96 <br /> Limits 81-120 82-112 85-112 83-113 <br /> "-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />