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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster,PA 176052425•717-656-2300 Fax 717-656-2681•www lanCaSterlabs com <br /> Page 3 of 3 49 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 656625 <br /> Reported=05/-29/03=at:310 38=PM <br /> Surrogate Quality Control <br /> Blank 91 <br /> LCS 90 <br /> LCSD 89 <br /> MS 88 <br /> Limits 57-146 <br /> Analysis Name BTEX + Oxygenates by 8260B <br /> Batch number P031762AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4068531 104 105 101 92 <br /> 4068532 104 104 100 92 <br /> 4068533 102 102 101 96 <br /> 4068534 103 106 102 93 <br /> 4068535 102 106 102 94 <br /> 4068536 102 103 101 92 <br /> 4068537 103 103 101 91 <br /> Blank 104 104 103 94 <br /> LCS 103 102 99 96 <br /> MS 101 105 100 99 <br /> MSD 101 104 99 98 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX + Oxygenates by 8260E <br /> Batch number P031771AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4068538 98 99 99 94 <br /> 4068539 98 97 100 93 <br /> Blank 96 96 100 94 <br /> LCS 95 100 97 97 <br /> MS-9 99 97 98 <br /> MSE) 96 96 97 97 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX + Oxygenates by 82608 <br /> Batch number P031791AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4068540 96 96 97 93 <br /> Blank 97 91 99 93 <br /> LCS 97 94 97 100 <br /> MS 98 89 97 99 <br /> MSD 96 91 95 99 <br /> Limits 81-120 62-112 85-112 83-113 <br /> *- Outside of specification <br /> (l) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />