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Mar-31-03 08 09am From-Gettlar-Ryan Inc +925 551 7899 T-365 P 026/029 F-412 <br /> Lancaster <br /> Laboratories Analysis Report <br /> sw Houand Pke.PO Bax 12-425 LoMasler PA 17605-2425•717.656-2300 Fax 717-656-2581-www.lanmsterlabs com <br /> Page ] of 3 <br /> Quality Control Summary <br /> Client Mame CbevronTexaco Group Number 845425 <br /> Reported 03/24/03 at 1.2 48 PM <br /> Laboratory Compliance Quality Control <br /> Dial* Blank Report LC5 LCSD LCS/LCSD � <br /> Amalvaxn Name Result M& units %AEC $Rgr- Liml& RPD Bpi) M <br /> Batch Number 03082A16A Sample number(S) 4014591-4014600 <br /> TPH-GRO - waters N D 54 ug/l 111 109 70-130 3 30 <br /> Batch number P03o601AA Sample number(a) 4014591-4014599 <br /> Methyl Tertiary Butyl Ether N D 5 ug/l 103 77-127 <br /> di-Isopropyl ether N D 5 ug/1 77 74-Z25 <br /> Ethyl t-butyl ether N D 5 ug/1 87 74-120 <br /> t-Amyl methyl ether N D 5 ug/1 99 79-113 <br /> t-Butyl alcohol N D 5 ug/1 99 53-147 <br /> BenzenC N D 5 ug/1 96 85-117 <br /> 1 2-Dichloroethane 1v b 5 ug/1 107 77-132 <br /> Toluene N D 5 ug/1 99 65-115 <br /> 1 2-Dibromoethane N D 5 ug/l 98 61--114 <br /> Ethylbenzene N D S u9/1 99 82-119 <br /> Xylene JTOCal) N D 5 u9/1 94 84-120 <br /> Batch number P030821AA sample number(s) 4014600 <br /> Methyl Tertiary Butyl Ethcr N D 5 ug/1 105 77-127 <br /> di-Isopropyl ether N 1) 5 ug/1 79 74-125 <br /> Ethyl t-butyl ether N D 5 ug/l 92 74-120 <br /> t-Amyl methyl ether N D 5 u9/1 104 79-113 <br /> cyl. alcohol N D 5- ug/l 99 53-147 <br /> enc N D 5 ug/1 96 85-117 <br /> Dichloroethane N D S ug/1 113 77-132 <br /> Toluene N A 5 ug/l 97 85-115 <br /> 1 2-Dxbromdethane N D 5 ug/1 97 61-114 <br /> EChylbenzene t3 D 5 ug/l 102 62-119 <br /> Xylene (Total) N D 5 ug/l 91 84-120 <br /> Sample Matrix Quality Control <br /> >!SS cf5p riS/>wi,SP RPD r:MG vur DUP Dup <br /> RPD <br /> sus Nam <br /> %RIELC }REC Lxiedrs RPD MX 22ne Conc RPD <br /> Batch number 03082AIGA Sample numbcr(S) _ 4014591-4014600 <br /> TPH-GRO - waters 120 70-130 <br /> Batch number P0308DIAA Sample number(s) - 4014591-4014599 <br /> Methyl Tertiary Butyl Ether 106 l09 69-334 3 30 <br /> di-zaopropyl ether 82 82 75-130 0 30 <br /> Ethyl r--butyl ether 90 91 73-123 1 30 <br /> t-Amyl methyl ether 107 105 77-117 1 30 <br /> t-Butyl alcohol 105 106 39-155 1 30 <br /> Benzene 101 102 83-129 1 30 <br /> 1,2-Dichloroethane 112 113 73-136 1 30 <br /> Toluene 107 109 e3-127 2 30 <br /> 1,2-Dibromaethane 97 102 78-120 5 30 <br /> Ethylbenzene 105 105 82-134 0 30 <br /> Xylmne (Total) 100 99 92-130 1 30 <br /> Batch number P030822AA Sample numbers) 4014600 <br /> Methyl Tertiary Butyl Ether 106 107 69-134 1 30 <br /> di-Isopropyl ether 79 79 75-130 1 30 <br /> *-Outside of specification <br /> (l) The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br />