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1534 Willow Pass Road,Pittsburg,CA 94565.1701 <br /> M c C a m p b e I l Analytical, I n c. Toll Free Telephone:(877)252-9242/Fax:(925)252-9269 <br /> ✓ „When Quality Counts" http:/lv vw.tnccampbell.cpm/E-mail:main@mccampbell.com <br /> Quality Control Report <br /> Client: Ponder Environmental Services WorkOrder: 1701 D08 <br /> Date Prepared: 1130117 BatchlD: 133373 <br /> Date Analyzed: 1/31/17 Extraction Method: SW3550B <br /> Instrument: GC17 Analytical Method: SW8270C <br /> Matrix: Soil Unit: mg/Kg <br /> Project: 17-16039; Pacific Ethanol Spill Sample ID: MB/LCS-133373 <br /> 1701 C84-001 AMS/MSD <br /> QC Summary Report for SW8270C <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Result Result Val %REC /REC Limits <br /> Acenaphthene NO 3.95 0.25 5 79 46-118 <br /> Acenaphthylene NO 0.25 <br /> Acetochlor NO 0.25 <br /> Anthracene ND - 0.25 <br /> Benzidine NO <br /> Benzo(a)anthracene NO 0.25 - <br /> Benzo(a)pyrene NO 0.25 - <br /> Benzo(b)fluoranthene NO - 0.25 - <br /> Benzo(g,h,i)perylene NO 0.25 <br /> Benzo(k)fluoranthene-- -- NO 0.25 - - <br /> Benzyl Alcohol NO 1.3 <br /> 1,1-Biphenyl ND 0.25 - - <br /> Bis(2-chloroethoxy)Methane NO 0.25 - <br /> Bis(2-chloroethyl)Ether NO 0.25 - <br /> Bis(2-chloroisopropyl)Ether NO - 0.25 - - - <br /> Bis(2-ethylhexyl)Adipate NO - 0.25 - <br /> Bis(2-ethylhexyl)Phthalate NO - 0.25 <br /> 4-Bromophenyl Phenyl Ether NO - 0.25 - <br /> Butylbenzyl Phthalate ND - 0.25 - - <br /> 4-Chloroaniline NO - 0.50 - - <br /> 4-Chloro-3-methylphenol NO 4.10 0.25 5 82 49-123 <br /> 2-Chlor)naphthalene NO - 0.25 - - - <br /> 2-Chlorophenol NO 4.30 0.25 5 86 55-116 <br /> 4-Chlorophenyl Phenyl Ether NO - 0.25 - <br /> Chrysene NO - 0.25 - - - - <br /> Dibenzo(a,h)anthracene NO 0-25 - <br /> Dibenzofuran NO - 0.25 - <br /> Di-n-butyl Phthalate NO 0.25 - - - <br /> 1,2-Dichlorobenzene NO - 0.25 - - - <br /> 1,3-Dichlorobenzene NO - 0.25 - - <br /> 1,4-Dichlorobenzene NO 3.81 0.25 5 - 76 50102 <br /> 3,3-91chlorobenzidine ND - 0.50 - - - <br /> 2,4-Dichlorophenel ND - 0.25 - - <br /> Diethyl Phthalate NO 0.25 - - <br /> 2,4-Dimethylphen01NO - 0.25 - <br /> Dimethyl Phthalate NO 0.25 - <br /> 4,6-Dinitro-2-methyiphenol NO 1.3 <br /> (Cont.) <br /> NELAP 4033ORELAP QAJQC Officer <br /> Page 46 of 69 <br />