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1534 Willow Pass Road,Pittsburg,CA 94565.1701 <br /> ±_ McCampbell Analytical, Inc. Toll Free Telephone:(877)252-9262 1 Fax:(925)252-9269 <br /> ti "When Quality Counts" littp://www.mccaanpbell.com/E-mail:mainr@imccampbell.com <br /> Quality Control Report <br /> Client: Ponder Environmental Services WorkOrder: 1701D08 <br /> Date Prepared: 1130117 BatchID: 133375 <br /> Date Analyzed: 1/31/17 Extraction Method: E625 <br /> Instrument: GC21 Analytical Method: SW8270C <br /> Matrix: Water Unit: µg/L <br /> Project: 17-16039; Pacific Ethanol Spill Sample ID: MB/LCS/LCSD-133375 <br /> QC Summary Report for SW8270C <br /> Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD <br /> Result Result Val %REC %REC Limits Limit <br /> Acenaphthene 9.82 10.7 10 98 107 47-145 8.81 20 <br /> 4-Chloro-3-methylphenol 8.61 9.28 10 86 93 22-147 7.44 20 <br /> 2-Chlorophenol 8.56 9.45 10 86 94 23-134 9.89 20 <br /> 1,4-Dichlorobenzene 7.71 8.59 10 77 86 20-124 10.8 20 <br /> 2,4-Dinitrotoluene 10.0 11.4 10 100 114 39-139 13.0 20 <br /> 4-Nitrophenol 57.6 58.5 50 115 117 1-132 1.64 20 <br /> N-Nitrosodi-n-propylamine 9.53 10.5 10 95 105 1-230 9.37 20 <br /> Pentachlorophenol 17.8 19.2 20 89 96 14-176 7.84 20 <br /> Phenol 9.40 10.0 10 94 100 5-112 6.59 20 <br /> Pyrene 8.57 10.0 10 86 100 52-115 15.5 20 <br /> 1,2,4-TrichIoro benzene 7.71 8.54 10 77 85 44-142 10.2 20 <br /> Surrogate Recovery <br /> 2-Fluorophenol 13.5 15.6 20 67 78 29-140 14.5 20 <br /> Phenol-d5 15.9 18.2 20 80 91 38-148 13.2 20 <br /> Nitrobenzene-d5 13.7 15.4 20 68 77 31-152 11.9 20 <br /> 2-Fluorobiphenyl 13.4 14.7 20 67 74 40-140 9.36 20 <br /> 2,4,6-Tribromophenol 13.4 14.2 20 67 71 39-150 5.75 20 <br /> Terphenyl-d14 12.0 14.0 20 60 70 38-147 15.9 20 <br /> NELAP 4033ORELAP QA/QC Officer <br /> Page 51 of 69 <br />