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d 1534 Willow Pass Road,Pihsbnrg,CA 94565-1701 Mccampbell Analytical, Inc. ToNFree Telephonc:(877)252.9262/Fax:(925)252-9269 "When Quality Counts" http:/hwww.mccampbell com/E-mail:main t�i nccmnpbeIl.com Quality Control Report Client: Ponder Environmental Services Work©rder: 1701D08 Date Prepared: 1/30/17 8atchlD: 133350 Date Analyzed: 1130/17-2/1/17 Extraction Method: SW5030B Instrument: GC10 Analytical Method: SW8260B Matrix: Soil Unit: mg/kg Project: 17-16039;Pacific Ethanol Spill Sample ID: MB/LCS-133350 1701 C 84-001 AMS/MSD QC Summary Report for SW8260B Analyte MB LCS RL SPK MB SS LCS LCS Result Result Val %REC %REC Limits 1,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND - 0.0050 - - trans-1,3-Dichloropropene ND - 0.0050 - Diisopropylether(DIPE) ND 0.0501 0.0050 0.050 - 100 52-129 Ethylbenzene ND - 0.0050 - - - - Ethyl tert-butyl ether(ETBE) ND 0.0524 0.0050 0,050 105 53-125 Freon 113 ND - 0.0050 - - - - Hexachlorobuladiene ND - 0.0050 - Hexachloroethane ND - 0.0050 - - 2-Hexanone ND - 0.0050 - - - Isopropylbenzene ND - 0.0050 - 4-Isopropyl toluene ND - 0.0050 - - Methyl-t-butyl ether(MTBE) ND 0.0523 0.0050 0.050 - 105 58-122 Methylene chloride ND - 0.0050 - - - - 4-Methyl-2-pentanone(MIBK) ND 0.0050 - Naphthalene ND - 0.0050 - - n-Propyl benzene ND - 0.0050 - Styrene ND 0.0050 - 1,1,1,2-Tetrachloroethane ND - 0,0050 - - 1,1,2,2-Tetrachloroethane ND - 0.0050 - - Tetrachloroethene ND - 0.0050 - - Toluene ND 0.0557 0.0050 0.050 111 76-130 1,2,3-Trichlorobenzene ND - 0.0050 - - - 1,2,4-Trichlorobenzene ND - 0.0050 - - - 1,1,1-Trichloroethane ND - 0.0050 - 1,1,2-Trichloroethane ND - 0.0050 - - - - Trichloroethene ND 0.0519 0.0050 0.050 - 104 72-132 Trichlorofluoromethane ND - 0.0050 - - - 1,2,3-Trichloropropane ND - 0.0050 - - - 1,2,4-Trimethylbenzene ND - 0.0050 - - 1,3,5-Trimethylbenzene ND - 0.0050 - - Vinyl Chloride ND - 0.0050 - Xylenes,Total ND - 0.0050 - (Cont,) NELAP 4033ORELAP " QA/QC Officer Page 38 of 69