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McCam bell Analytical Inc. 1534 willow Pass Road,Pittsburg,CA 94565-1701 <br /> f- Tall Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Qualki,Counts" http://www.mccampbell.com/E-mail:mfdn@mccaiiipbell.com <br /> Quality Control Report <br /> Client: Ponder Environmental Services WorkOrder: 17011308 <br /> Date Prepared: 1/30/17 BatchlD: 133385 <br /> Date Analyzed: 1/30/17 Extraction Method: SW5030B <br /> Instrument: GC16 Analytical Method: SW8260B <br /> Matrix: Water Unit: pg/L <br /> Project: 17-16039;Pacific Ethanol Spill Sample ID: MB/LCS-133385 <br /> 1701 C34-004AMS/MSD <br /> QC Summary Report for SW8260B <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Result Result Val %REG %REC Limits <br /> Acetone ND 10 - <br /> tert-Amyl methyl ether(TAME) NO 7.68 0.50 10 77 54-140 <br /> Benzene NO 9.14 0.50 10 91 47-158 <br /> Bromobenzene NO - 0.50 - - - <br /> Bromochloromethane NO 0.50 - - <br /> Bromodichloromethane NO 0.50 - - - <br /> Bromoform NO 0.50 _ _ <br /> Bromomethane NO - 0.50 _ - <br /> 2-Butanone(MEK) NO - 2.0 - - - - <br /> t-Butyl alcohol(TBA) NO 24.9 2.0 40 - 62 42-140 <br /> n-Butyl benzene NO - 0.50 - - - - <br /> sec-Butyl benzene NO - 0.50 - <br /> tert-Butyl benzene NO _ 0.50 - - <br /> Carbon Disulfide NO 0,50 _ <br /> Carbon Tetrachloride NO - 0.50 - - - <br /> Chlorobenzene NO 9.10 0.50 10 - 91 43-157 <br /> Chloroethane NO - 0.50 - - - <br /> Chloroform NO 0.50 - <br /> Chloromethane NO - 0.50 - <br /> 2-Chlorotoluene NO - 0.50 _ <br /> 4-Chlorotoluene NO - 0.50 - <br /> Dibromochloromethane NO 0.50 - <br /> 1,2-Dbromo-3-chloropropane NO - 0,20 - _ <br /> 1,2-Dibromoethane(EDB) NO 8.41 0.50 10 84 44-155 <br /> Dibromomethane NO - 0.50 _ _ <br /> 1,2-Dichlorobenzene NO - 0.50 _ <br /> 1,3-Dichlorobenzene ND - 0.50 - <br /> 1,4-Dichlorobenzene NO - 0.50 - <br /> Dichlorodifluoromethane NO - 0.50 _ <br /> 1,1-Dichloroethane NO - 0,50 _ <br /> 1,2-Dichloroethane(1,2-DCA) NO 8.01 0.50 10 80 66-125 <br /> 1,1-Dichloroethene NO 9.07 0.50 10 - 91 47-149 <br /> cis-1,2-Dichloroethene NO - 0.50 - - - - <br /> trans-1,2-Dichloroethene ND 0.50 _ <br /> 1,2-Dichloropropane NO - 0.50 - - <br /> 1,3-Dichloropropane ND _ 0.50 - _ <br /> 2,2-Dichloropropane NO 0.50 _ _ <br /> (Cont.) <br /> NELAP 4033ORELAP L- - <br /> QA/QC Officer <br /> Page 43 of 69 <br />