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QC Sample Results <br /> Client: Dysert Environmental, Inc TestAmerica Job 10: 720-86460-1 <br /> Project/Ste: Zega Building <br /> Method: 82608 -Volatile Organic Compounds (GCiMS) (Continued) <br /> Lab Sample ID: 720-86460-10 MS Client Sample ID: 53-6' <br /> Matrix: Solid Prep Type: TotallNA <br /> Analysis Batch: 244496 Prep Batch: 244270 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,1,2-Tetrachloroethane ND 49.8 56.4 ug/Kg 113 64.133 <br /> 1,1,2,2-Tetrachloroethane ND 49.8 55.1 ug/Kg 111 70-131 <br /> Tetrachloroethene ND 49.8 56.4 ug/Kg 113 67-130 <br /> Toluene ND 49.8 50.9 ug/Kg 102 70-130 <br /> 1,2,3-Trichlorobenzene ND 49.8 49.6 ug/Kg 100 58-138 <br /> 1,24-Trichlorobenzene ND 49.8 49.5 ug/Kg 99 49-144 <br /> 1,1,1-Trichloroethane ND 49.8 56.4 ug/Kg 113 57_133 <br /> 1,1,2-Trichloroethane ND 49.8 55.5 ug/Kg 111 68-132 <br /> Trichloroethene ND 49.8 53.8 ug/Kg 108 66-130 <br /> Trichlorofluoromethane ND 49.8 58.7 uglKg 118 61-130 <br /> 1,2,3-Trichloropropane ND 49.8 56.0 ug/Kg 113 62-150 <br /> 1,1,2-Trichloro-1,2,2-tdfluoroetha ND 49.8 60.6 ug/Kg 122 52-130 <br /> ne <br /> 1,2,4-Tdmethylbenzene ND 49.8 54.4 ug/Kg 109 64-140 <br /> 1,3,5-Tri methyl benzene ND 49.8 54.5 ug/Kg 109 67-134 <br /> Vinyl acetate ND 49.8 32.1 ug/Kg 64 52-150 <br /> Vinyl chloride ND 49.8 55.1 ug/Kg 111 62-130 <br /> m-Xylene&p-Xylene ND 49.8 53.0 ug/Kg 106 70-130 <br /> o-Xylene ND 49.8 51.6 ug/Kg 104 68-130 <br /> Xylenes,Total ND 99.6 105 ug/Kg 105 70-130 <br /> 2,2-Dichloropropane ND 49.8 53.9 ug/Kg 108 63-130 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Sromofluorobenzene 94 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 101 60-140 <br /> Toluene-d8(Surr) 102 58-140 <br /> Lab Sample ID: 720-86460-10 MSD Client Sample ID: S3-6` <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 244496 Prep Batch: 244270 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Methyl tert-butyl ether ND 49.8 54.5 ug/Kg 109 69-130 4 20 <br /> Acetone ND 249 261 ug/Kg 105 37-150 3 20 <br /> Benzene ND 49.8 51.6 ug/Kg 104 70-130 5 20 <br /> Dichlorobromomethane ND 49.8 52.6 ug/Kg 106 64-135 6 20 <br /> Bromobenzene ND 49.8 50.4 ug/Kg 101 70-130 7 20 <br /> Chlorobromomethane ND 49.8 54.0 ug/Kg 108 65-130 7 20 <br /> Bromoform ND 49.8 54.6 ug/Kg 110 58-132 1 20 <br /> Bromomethane ND 49.8 57.0 ug/Kg 114 56-130 4 20 <br /> 2-Butanone(MEK) ND 249 250 ug/Kg 100 41-150 2 20 <br /> n-Butylbenzene ND 49.8 49.1 ug/Kg 99 60-145 5 20 <br /> see-Butylbenzene ND 49.8 51.9 uglKg 104 64-137 5 20 <br /> tert-Butylbenzene ND 49.8 52.3 ug/Kg 105 63-134 5 20 <br /> Carbon disulfide ND 49.8 51.8 ug/Kg 104 10-150 6 20 <br /> Carbon tetrachloride ND 49.8 55.9 ug/Kg 112 54-130 4 20 <br /> Chlorobenzene ND 49.8 49.9 ug/Kg 100 70-130 3 20 <br /> Chloroethane ND 49.8 52.9 ug/Kg 106 M-130 2 20 <br /> TestAmerica Pleasanton <br /> Page 33 of 75 5/21/2018 <br />