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Page 10 of 21 <br /> alscience <br /> i nvironmental Quality.Control- Spike/Spike Duplicate <br /> aboratories, Inc. <br /> Shell Oil Pipeline Company LP Date Received: 10/21/08 <br /> P.O. Box 2648 Work Order No: 08-10-1847 <br /> Houston, TX 77252-2648 Preparation: EPA 50308 <br /> Method: EPA 8260E <br /> Project 25705 Patterson Pass Rd., Tracy, CA <br /> Date Date MS/MSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> X06-10-2156-1MumSolid GGlM5_XX 10!28!08 10!26108, 081028501 <br /> Parameter MS%REC MSD%REC %REC CL RPD RPD CI_ Qualifiers <br /> Benzene 90 87 79-115 4 0-13 <br /> Carbon Tetrachloride 88 82 55-139 7 0-15 <br /> Chlorobenzene 89 85 79-115 5 0-17 <br /> 1,2-Dibromoethane 94 95 70-130 1 0-30 <br /> 1,2-Dichlorobenzene 87 85 63-123 3 0-23 <br /> 1,1-Dichloroethene 70 60 69-123 16 0-16 3 <br /> Ethylbenzene 90 85 70-130 6 0-30 <br /> Toluene 89 86 79-115 4 0-15 <br /> Trichloroethene 88 85 66-144 4 0-14 <br /> Vinyl Chloride 68 68 60-126 1 0-14 <br /> Methyl-t-Butt'!Ether(MTBE) 105 104 68-128 1 0-14 <br /> Tert-Butyl Alcohol(TBA) 127 132 44134 4 0-37 <br /> Diisopropyl Ether(DIPE) 95 92 75-123 3 0-12 <br /> Ethyl-t-Butyl Ether(ETBE) 102 99 75-117 3 0-12 <br /> Tert-Amyl-Methyl Ether(TAME) 100 101 79-115 1 0-12 <br /> Ethanol 63 72 42-138 13 0-28 <br /> RPD-Relative Peroent DifferEnce, C�•Control Limit <br /> 7440 Lincoln Way, Garden.Grove, CA 92841-1427 . TEL:(714)895-5494 • FAX: (714)894-7501 <br />