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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax :925-798-1622 <br /> 24 http://www.mccampbell.com E-mail:main@mccwnpbell.com <br /> Advanced GeoEnvironmental Client Project ID:Western Square Date Sampled: 09/07/99 <br /> 4005 North Wilson Way Industries Date Received: 09/10/99 <br /> Stockton,CA 95205 Client Contact:Robert Marty Date Extracted: 10/20/99 <br /> Client P.O: Date Analyzed: 10/20-10/21/99 <br /> Metals* <br /> EPA methods 60101200.7;7470174711245.11245.5(Hg);7060/206.2(As);77401270.2(Se);7841/279.2(11);239.2(Pb,water matrix) <br /> Lab ID 18978 18979 <br /> Reporting Limit <br /> Client ID SP-1-2 SP-3-4 <br /> Matrix S S S W STLC, 4 <br /> TCLP <br /> Extraction' TTLC TTLC TTLC TTLC <br /> Compound Concentration* mg/kg mg/L mg/L <br /> Antimony(Sb) ND ND 2.5 0.05 0.05 <br /> Beryllium(Be) ND 0.51 0.5 0.004 0.01 <br /> Cobalt(Co) 13 13 2.0 0.05 0.05 <br /> Copper(Cu) 110 57 2.0 0.05 0.05 <br /> Molybdenum(Mo) 630 280 2.0 0.05 0.05 <br /> Nickel(Ni) 49 55 2.0 0.05 0.05 <br /> Thallium(Tl) ND ND 2.5 0.005 0.5 <br /> Vanadium(V) 51 69 2.0 0.05 0.05 <br /> Zinc(Zn) 240 120 1.0 0.05 0.05 <br /> %Recovery Surrogate 102 105 <br /> Comments <br /> • water samples are reported in mg/L,soil and sludge samples in mgtkg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> EPA extraction methods 1311(TCLP),301013020(water,TTLC),3040(organic matrices,T"Tl-C),3050(solids,TTLC);STLC-CA Title 22 <br /> 'surrogate diluted out of range <br /> a reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than -2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 �� � Edward Hamilton, Lab Director <br />