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O V A L 1. I .Y . A S S.U R A N 'C E.,. .,.M. E T fl,.p.,g . . . .
<br /> R,.E. I=,.E. R..E N C E. S A N;,.D .N:p T F:.S., . . . .
<br /> Report Date.,Q6/23/2003
<br /> REPORT COMMENTS
<br /> 1) All pages of this report are integral parts of the analytical data. Therefore, this report should
<br /> be reproduced only in its entirety.
<br /> 2) soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for
<br /> landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as
<br /> received" basis unless noted differently.
<br /> 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
<br /> 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201
<br /> 5) Arizona Environmental Laboratory License number AZ0603.
<br /> 6) According to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved oxygen analyses are to be performed
<br /> immediately after aqueous sample collection. When these parameters are not indicated as field (e.g.
<br /> pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt.
<br /> Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report)
<br /> Inorganic Qualifiers (0-Column)
<br /> U Analyte was not detected at or above the stated limit.
<br /> c Not detected at or above the reporting limit_
<br /> J Result is less than the RL, but greater than or equal to the method detection limit.
<br /> B Result is less than the CROL/RL, but greeter than or equal to the IDL/MDL.
<br /> S Result was determined by the Method of standard Additions.
<br /> F AFCEE: Result is less than the RL, but greater than or equal to the method detection limit,
<br /> lnarganic Flags (F(ag Column)
<br /> ICV,CCV,ICB,CCB,I5A,1sB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower
<br /> control limits.
<br /> * LCS, LCD, MD; Batch 4C exceeds the upper or lower control limits.
<br /> + MSA correlation coefficient is less than 0.445.
<br /> 4 Ms, MSD; The analyte present in the original sample is 4 times greater
<br /> than the matrix spike concentration; therefore, control limits are not applicable.
<br /> E BD: Serial dilution exceeds the control Limits.
<br /> H MB, E81, ES2, EB3: Batch OC is greater than reporting limit or had a
<br /> negative instrument reading lower than the absolute value of the reporting limit.
<br /> N MS, MSD: spike recovery exceeds the upper or lower control limits_
<br /> w AS(GFAA) Post-digestion spike was outside 85-115% control limits.
<br /> Organic Qualifiers (Q - Column?
<br /> u Analyte was not detected at or above the stated limit.
<br /> ND Compound not detected.
<br /> J Result is an estimated value below the reporting limit or a tentatively
<br /> identified compound (TIC).
<br /> ❑ Result was qualitatively confirmed, but not quantified.
<br /> C Pesticide identification was confirmed by GC/Ms.
<br /> Y The chromatographic response resembles a typical fuel pattern_
<br /> Z The chromatographic response does not resemble a typical fuel pattern.
<br /> E Result exceeded calibration range, secondary dilution required,
<br /> F AFCEE:Result is an estimated value below the reporting limit or a tehtativeLy identified compound (TIC)
<br /> Organic Flags (Flags Column)
<br /> B MB. Batch QC is greator than reporting limit.
<br /> * LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits.
<br /> EB1, EB2, EB3, MLE: Batch QC is greater than reporting Limit
<br /> A Concentration exceeds the instrument calibration range
<br /> a Concentration is below the method Reporting Limit (RL)
<br /> B Compound was found in the blank and sample.
<br /> D Surrogate or matrix spike recoveries were not
<br /> obtained because tho extract was diluted for
<br /> analysis; also compounds analyzed at a dilution will be fLagged with a D.
<br /> H Alternate peak selection upon analytical review
<br /> I Indicates the presence of an interfence, recovery is not calculated.
<br /> M Manually integrated compound.
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