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. .. <br /> . <br /> 1:::.T:...Y �,4 $ $,'U R A N.::d M E T H';', <br /> . . ,. <br /> A,-N- D 4.0j.E::: ., ., <br /> REPORT COMMENTS <br /> 1) ALL pages of this report are integral parts of the analytical data. Therefore, this report should <br /> be reproduced only in its entirety. <br /> 2) SoiL, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for <br /> landfill disposal or incineration parameters. ALL other solid matrix samples are reported on an 'gas <br /> received" basis unless noted differently. <br /> 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. <br /> 4) The test resuLts for the noted analytical method(s) meet the requirements of NELAG. Lab Cert. I0# 100201 <br /> 5) Arizona Environmental Laboratory License number AZ0603. <br /> 6) According to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed <br /> immediately after aqueous sample collection. When these parameters are not indicated as field (e,g. <br /> pH Field) they were not analyzed immediately, but as soon as possible on Laboratory receipt. <br /> Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) <br /> inorganic Qualifiers (GM-Column) <br /> U Analyte was not detected at or above the stated limit. <br /> Not detected at or above the reporting limit. <br /> J Result is Less then the RL, but greater than or equal to the method detection limit. <br /> B Result is less than the CRDLIRL, but greater than or equal to the IDL/MDL. <br /> S Result was determined by the Method of Standard Additions. <br /> F AFCIE: Result is less than the RL, but greater than or equal to the method detection Limit. <br /> inorganic Flags (Flag Column) <br /> ICV,CCV,ICB,CCB,ISA,ISB,CRI,CRA,MRL: Instrument related 4C exceed the upper or lower <br /> control limits. <br /> * LCS, 4CD, MD: Batch QC exceeds the upper or Lower control limits. <br /> + MSA correlation coefficient is less than 0.995. <br /> 4 ME, MSD: The analyte present in the original sample is 4 times greater <br /> than the matrix spike concentration; therefore, control limits are not appLicable. <br /> E SO: Serial dilution exceeds the control limits. <br /> H MB, E81, E82, ER3: Batch X is greater than reporting limit or had a <br /> negative instrument reading lower than the absolute value of the reporting limit. <br /> N ME, MSD: Spike recovery exceeda the upper or lower control limits. <br /> W AS(GFAA) Post-digestion spike was outside 85-115% control Limits. <br /> organic Qualifiers (0 - Column) <br /> u Analyte was not detected at or above the stated limit. <br /> ND Compound not detected. <br /> i Result is an estimated value below the reporting limit or a tentatively <br /> identified compound (TIC). <br /> Q Result was qualitatively confirmed, but not quantified. <br /> C Pesticide identification was confirmed by BE/M5_ <br /> Y The chromatographic response resembles a typical fuel pattern. <br /> 2 The chromatographic response does not resemble a typical fuel pattern- <br /> F; Result exceeded calibration range, secondary dilution required. <br /> F AFCEE:Result is an estimated value below the reporting limit or a tentatively identified compound (TIC) <br /> Organic Flags (Flags Column) <br /> B MB: Batch 4C is greater than reporting limit. <br /> * LCS, LCD, ELC, ELo, CV, ME, MSD, Surrogate: Batch 4C exceeds the upper or lower control limits. <br /> EB1, E82, E63, MLE: Batch GMC is greater than reporting Limit <br /> A Concentration exceeds the instrument calibration range <br /> a Concentration is below the method Reporting Limit (RL) <br /> B Compound was found in the blank and sample, <br /> D Surrogate or matrix spike recoveries were not <br /> obtained because the extract was diluted for <br /> analysis; also compounds analyzed at a dilution will be flegged with a D. <br /> H Alternate peak selection upon analytical review <br /> I Indicates the presence of an interfence, recovery is not calculated. <br /> M Manually integrated compound_ <br /> Page 8 <br />