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., .... -------- <br /> 4 U L .1 T. Y A S. g.0 R A N .0 E M E T 8 0 D. S. . . <br /> R E F E R E. N' C E A N D N 0' T E S <br /> Report Datec 06)Z3/2Q.Q3 <br /> REPORT COMMENTS <br /> 1) All pages of this report are integral parts of the analytical data. Therefore, this report should <br /> be reproduced only in its entirety. <br /> 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for <br /> Landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as <br /> received" basis unless noted differently. <br /> 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. <br /> 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 <br /> 5) Arizona Environmental Laboratory License number A20603. <br /> 6) According to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed <br /> immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. <br /> pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt. <br /> Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) <br /> Inorganic Qualifiers (4-Column) <br /> U Analyte was not detected at or above the stated limit. <br /> < Not detected at or above the reporting limit. <br /> J Result is less than the RL, but greater than or equal to the method detection limit. <br /> B Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. <br /> 5 Result was determined by the Method of Standard Additions. <br /> F AFCEE: Resutt is less than the RL, but greater than or equal to the method detection limit. <br /> Inorganic Flags (Flag Column) <br /> ICV,CCV,ICB,CCB,ISA,i$B,CRI,CRA,MRL: Instrument related dC exceed the upper or lower <br /> control limits. <br /> LC5, LCD, MO: Batch 4C exceeds the upper or loner control limits. <br /> + MSA correlation coefficient is less than 0.445- <br /> 4 M5, MSD: The analyte present in the original sample is 4 times greater <br /> than the matrix spike concentration; therefore, control Limits are not applicable. <br /> E SD: serial dilution exceeds the control limits, <br /> H MB, E81, E82, E133: Batch 4C is greater than reporting limit or had a <br /> negative instrument reading lower than the absolute value of the reporting limit. <br /> N MS, MSD: Spike recovery exceeds the upper or Lower control limits. <br /> w AS(GFAA) post-digestion spike was outside 85.115% control limits. <br /> Organic Qualifiers (0 - Column) <br /> U Analyte was not dotected at or above the stated limit. <br /> ND Compound not detected. <br /> J Result is an estimated value below the reporting limit or a tentatively <br /> identified compound (TIC). <br /> 4 Result was qualitatively confirmed, but not quantified. <br /> C Pesticide identification was confirmed by GC/MS. <br /> Y The chromatographic response resembles a typical fuel pattern. <br /> 2 The chromatographic response does not resemble a typical fuel pattern. <br /> E Result exceeded calibration range, secondary dilution required. <br /> F AFCEE!Result is an estimated value below the reporting limit or a tentatively identified compound (TIC) <br /> Organic Flags (Flags Column) <br /> E MB: Batch QC is greater then reporting limit. <br /> * LCs, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower Control limits. <br /> EBI, E82, CB3, MLE: Batch QC is greater then reporting Limit <br /> A Concentration exceeds the instrument calibration range <br /> a Concentration is below the method Reporting Limit (RL) <br /> 6 Compound was found in the blank and sample. <br /> D Surrogate or matrix spike recoveries were not <br /> obtained because tht extract was diluted for <br /> analysis; also compounds analyzed at a dilution will bt flagged with a D. <br /> H Alternate peak selection upon analytical review <br /> I Indicates the presence of an interfence, recovery is not calculated. <br /> M ManuaLLy integrated Compound, <br /> Page 8 <br />