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0 U A L. 1 T YA.S S U R. A. N. C I H E T H 0 O S. . <br /> R E F E R' E N C E S A'.N,;D ';.' N;0 r .E g,., <br /> R6port::Date;; 06/:27/2.003 <br /> REPORT COMMENTS <br /> 1) All pages of this report are integral parts of the analytical data. Therefore, this report should <br /> be reproduced only in its entirety. <br /> 2) Soit, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for <br /> landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as <br /> received" basis unless noted differently. <br /> 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. <br /> 4) The test results for the noted analytical meth❑d(s) meet the requirements of NELAC. Lab Cert. 1D# 100201 <br /> 5) Arizona Environmental Laboratory License number A20603. <br /> 6) According to 40EFR Part 1363, pH, Chlorine Residual and N 55citved Oxygen analyses are to be performed <br /> immediately after aqueous sample collection. when these parameters are not indicated as field (e.g. <br /> pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt. <br /> Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) <br /> Inorganic Qualifiers (Q-Column) <br /> U Analyte wag not detected at or above the stated limit. <br /> < Not detected at or above the reporting Limit. <br /> J Result is less than the RL, but greater than or equal to the method detection limit. <br /> B Result is less than, the CRDL/RL, but greater than or equal to the IDL/MDL. <br /> S Result was determined by the Method of Standard Additions. <br /> F AFCEE: Result is less than the RL, but greater than ❑r equal to the method detection limit. <br /> Inorganic Flags (Flag Column) <br /> ICV,CCV,ICB,CCB,ISA,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower <br /> control limit;;_ <br /> " LCS, LCD, MD: Batch QC exceeds the upper or Lower control limits. <br /> + MSA correlation coefficient is less than 0.445. <br /> 4 MS, MSD: The analyte present in the original sample is 4 times greater <br /> than the matrix spike concentration; therefore, control limits are not applicable. <br /> E SD: Seriat dilution exceeds the control limits. <br /> H MB, EB1, E82, EB3: Batch QC is greater than reporting Limit or had a <br /> negative instrument reeding lower than the absolute value of the reporting Limit. <br /> N MS, MSD: Spike recovrry exceeds the upper or lower control limits. <br /> W AS(GFAA) Past-digestion spike was outside 85-115% control Limits, <br /> organic Qualifiers (Q - Column) <br /> V Analyte was not detected at or above the stated limit. <br /> ND compound not detected_ <br /> .1 Result is an estimated value below the reporting limit or a tentatively <br /> identified compound (TIC)- <br /> 0 Result was qualitatively confirmed, but not quantified. <br /> C Pesticide identification was confirmed by GC/MS, <br /> Y The chromatographic response resembles a typical fuel pattern. <br /> Z The chromatographic response does not resemble a typical fuel pattern. <br /> E Result exceeded calibration range, secondary dilution required, <br /> F AFCEE:ResuLt is an estimated value below the reporting limit or a tentatively identified compound (TIC) <br /> Organic Flags (Flags Column) <br /> B MB: Batch 0C is greater than reporting limit. <br /> " LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits. <br /> EB1, EB2, EB3, ML5: Batch QC is greater than reporting Limit <br /> A Concentration exceeds the instrument calibration range <br /> a Concentration is below the method Reporting Limit (RL) <br /> B Compound was found in the blank and sample. <br /> D Surrogate or matrix spike recoveries were not <br /> obtained because the extract was diluted for <br /> analysis; also compounds analyzed at a dilution will be flagged with a D. <br /> H Alternate peak selection upon analytical review <br /> I Indicates the presence of an interfence, recovery is not calculated. <br /> M Manually integrated Compound. <br /> Page 8 <br />