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• i <br /> Entech Analytical Labs® Dncn <br /> 3334 Victor Court a Santa Clara, CA 95054 a (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Project Name: PG&E <br /> Benicia,CA 94510 Project Number: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-001 Client Sample ED: Bl-5 <br /> Sample Time: 8:50 AM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene ND 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Toluene ND 1 0.625 0.025 mgtkg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene ND I 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Xylenes,Total ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Contra)Limits(%) <br /> 4-Bramofluorobenzene 95.9 65 - 135 <br /> P:vaneter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPN as Diesel 3.3 x I 1 1 mg/Kg 3/13/2003 3/14/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 79.0 50 - 126 <br /> Comment: Not a TPH as Diesel pattern;Value due to overlap from the Motor Oil range into the Diesel quantitation range. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> 7PH as Gasoline ND 1 2.5 2.5 mg/kg 3114/2003 3/14/2003 SGC42784 EPA 8015 MOD. <br /> (Purgcable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-BromoOuorobenwric 92.0 65 - 135 <br /> Parunieter Resuh Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Till]as Motor Oil ND 1 13 13 mg/Kg 3/13/2003 3/142003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Tcrpheny) 79.0 40 - 128 <br /> DF-Dilution Faclor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical labs,Inc.(CA SLAP#2346) <br /> Patti Sandrock,QA/QC Manager Environmental Anal y-5is Since 1983 <br />