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A <br /> Entech Analytical Labs, Inca <br /> 3334 Victor Court a Santa Clara, CA 95054 a (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Benicia,CA 94510 Project Name: PG&E <br /> Project Number: 03400 00 <br /> Attu: Chris Bramer P.O.Number: 03400 00 <br /> Sampled Ey: Casey Poldino <br /> Certifier!Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-005 Client Sample ID: 135-6 <br /> Sample Time: 10:19 AM Sample Date: 3/13/2003 Matrix: Solid <br /> Par:uncur Result Flog DF PQL DLR Units Extraction Analysis y QC Botch ID Method <br /> Dote Date <br /> Benzene NO 1 0.025 0.025 mpkg 3/14/2003 3/1412003 SGC42784 EPA 8020 <br /> Toluene NO 1 0.025 0.025 mg/kg 3/1412003 3/14/2003 SGC42784 EPA 8020 <br /> Elbyl Benzene NO 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> xylenes,Total ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromolluorobenzone 97.7 65 - 135 <br /> i <br /> Parameter Result Flog DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Dale Date <br /> TPI I as Diesel 4.3 x I I I mg/Kg 3/13/2003 3/14/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits I[%) <br /> a-Terphonyl 08.0 50 - 120 <br /> Comment: Not a TPN as Diesel pattern;Value due to overlap from the I lydmulic Oil range into the Diesel quantitation range. '. <br /> Porumeter Result Flag DF PQL DLR Units Extraction Analysis QC Balch ID Method <br /> Dale Date <br /> TPI4 as Gasoline NO 1 2.5 2.5 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8015 MOD. <br /> (Purgeablc) <br /> Surrogate Surrogate Recovery Control Limlls(%) <br /> 4-Bromoguorobenzene 93.8 05 - 135 <br /> Parameter Result Flog DF PQL DLR Writs Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPIA as Motor Oil ND 1 13 13 mg/Kg 3/13/2003 3/14/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphcnyl 68.0 40 - 128 <br /> j <br /> OF=Dilution Factor ND Not Detected DLR-Detection Limit Reported PQL=Practical Quantilation Limit <br /> Analysis performed by Entech Analytical tabs,Inc.(CA FLAP 02340) <br /> �-fatti San rock,QA/QC Manager Environmental Analysis Since 1983 <br />