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9 0 <br /> Entech Ana yf cel Labs, Oman <br /> 3334 Victor Courto Santa Clara, CA 95054 • (408) 588-0200 e Fax (408) 588-0201 <br /> ECNI Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Project Name: PG&E <br /> Benicia,CA 94510 Project Number: 0340000 <br /> Attn: Chris Bremer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-009 Client Sample ID: B9-6 <br /> Sample Time: 11:05 AM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Butch ID Method <br /> Date Data <br /> Benzene ND 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 - <br /> Toluene NO 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene NO 1 0.025 0.025 mgfkg 3/1412003 3/14/2003 SGC42784 EPA 8020 <br /> xytenes,'roml ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromonuorobenzene 95.5 65 - 135 <br /> Parameter Result Flog DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPM as Diesel 2.3 x I i I mg/Kg 3/13/2003 3/14/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 68.0 50 - 126 <br /> Comment: Not a TPI I as Diesel pattern;Value due to overlap from the Motor Oil range into the Diesel quantitation range. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Butch ID Method <br /> Dale Date <br /> TPH us Gasoline NO 1 2.5 2.5 mg/kg 3/1412003 3/14/2003 SGC42784 EPA 8015 MOD. <br /> (Forgeable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromanuorobenzcne 91.3 65 - 135 <br /> Parameter Result Fin-, DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI-1 as Motor Oil ND 1 13 13 mg/Kg 3/13/2003 3/142003 DS4259A EPA 8615 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terplrenyl 68.0 40 - 128 <br /> DP=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quuntitnon Limit <br /> Analysis performed by Emech Analytical Labs,Inc.(CA ELAP#2346) <br /> -X —0 <br /> y/J <br /> Patti Sandrock,QA/QC Manager Environmental Analysis Since 1983 <br />