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9 0 <br /> Entech ,analytical Labs, Inco <br /> 3334 Victor Court a Santa Clara, CA 95054 e (408) 588-0200 o Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> BProject Name:PG&E <br /> Benicia,CA 94510 <br /> Project Number: 03400 00 <br /> Attn: Cbris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldim) <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-013 Client Sample ED: B12-6 <br /> Sample Time. 12:50 PM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene NO 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Toluene ND 1 0.025 0.025 mg/kg 31142003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene NO 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Xylenes,Total ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Br0monu0robenzcnc 96.1 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPU as Diesel ND I I I mg/Kg 3/13/2003 3/142003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(°/) <br /> o-Terphcnyl 62.0 50 - 126 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI I as Gasoline NO 1 2.5 2.5 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8015 MOD. <br /> (Purgeuble) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-BromoRuarobenzene 90.5 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Dale <br /> TPI-I as Molar Oil NO 1 13 13 mgfKg 3/13/2003 3/142003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogute Recovery Control Limits(%) <br /> a-Terphenyl 62.0 40 - 128 <br /> OF=Dilution Factor NO Not Detected DLR=Detection Limit Reported PQL=Practical Qanntitaimn Limit <br /> Analysis perrarmed by Emcch Analytical Labs,Inc.(CA EIRP 82346) <br /> Patti San rock QA/QC Manager Environmental Analysis Since 1983 <br />