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• <br /> Entech Anaiy ocal Labs, Inco <br /> 3334 Victor Court Santa Clara, <br /> CA 95054 a (408) 588-0200 o Fax (408) 588-0201 <br /> ECIVI Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Project Name:PG&E <br /> Benicia,CA 94510 <br /> ProjectNumber: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample IN 33648-016 Client Sample ID: B14-10 <br /> i <br /> Sample Time: 2:20 AM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result ring DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene ND 5 0.025 0.125 mg/kg 3/14/2003 311412003 SGC42784 EPA 8020 <br /> Toluene NO 5 0.025 0.125 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene NO 5 0.025 0.125 mgfkg 3/14/2003 3/1412003 SGC42784 EPA 8020 <br /> Xylenes,Total NO 5 0.05 0.25 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Contra]Limits(%) <br /> 4-BromoBuorobenzene 87.3 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI I as Diesel 140 -;. 5 1 5 mg/KS 3/13/2003 3/16/2003 DS4259A EPA8015MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 84.0 50 - 126 <br /> Comment: Not a TPH as Diesel pattern;Value due to an unkrun"hydrocarbon(CIO-C34),overlapping into the Diesel quantitation range. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPH us Gasoline 22 x 5 2.5 12.5 mg/kg 3/14/2003 3/1412003 SGC42784 EPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromulluorobenzene 108.8 65 - 135 <br /> Comment: Reported TPH as Gasoline value is the result of heavy end hydrocarbons within the TPH as Gasoline quantitation range but not <br /> typical of TPH as Gasoline. <br /> Parameter Result Flag DF PQL DLR Units Extrattion Analysis QC Dutch ID Method <br /> Date Date <br /> 'Fills as Motor Oil 160 x 5 13 65 mg/Kg 3/132003 3/1612003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> a-Terpheryl 84.0 40 - 128 <br /> Comment: Not a Motor Oil pattern;Value due to an unknown hydrocarbon(CIO-C34),overlapping into the Motor Oil qua elation range. <br /> DF=Dilution Factor NO-Not Detected DLR=Detection Limit Reported PQL=Practical Quanlimlion Limit <br /> Analysis performed by Enuch Analytical labs.Inc.(CA FLAP 92346) <br /> alti S d - QA/QCManager Environmental Analysis Since 7983 <br />