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s • <br /> Entech Analytical Labs, Inco <br /> 3334 Victor Court Santa Clara, CA 95054 m (408) 588-0200 • Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Benicia,CA 94510 Project Name:PG&E <br /> Project Number: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 0340000 <br /> Certified Analytical Report Sampled By: Casey Poldino <br /> Order Ill: 33648 Lab Sample ID: 33648-034 Client Sample ID: B 12 <br /> Sample Time: 1:00 AM Sample Date: 3/13/2003 Matrix: Liquid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Dale <br /> Benzene NO 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Toluene ND 1 0.5 0.5 pg/L N/A 3/14/2003 WOC62783 EPA 8020 <br /> Ethyl Benzene ND 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> xylenes,Total NO 1 1 I pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromotluombenzene 104.6 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Botch 2D Method <br /> Date Date <br /> TPl I as Diesel 260 x 1 59 59 pg/L 3/14/2003 3/17/2003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 82.0 21 - 142 <br /> Comment: Reporting limit increased due to limited sample volume. Not a TPH as Diesel pattern;Value due to overlap from the Hydraulic Oil <br /> range and,discrete peals in the Diesel quantitation range. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Melhad <br /> Date Date <br /> TPH as Gasoline ND I 50 50 pg/L N/A 3/14/2003 14GC62783 EPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromonuombenzene 90.8 65 - 135 <br /> Parameter Result Flog DF PQL DLR Units Extraction Analysis QC Batch lD Method <br /> Date Date <br /> TPH as Motor Oil NO 1 294 294 pg/L 3/14/2003 3/17/2003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> o-Terphertyl 82.0 32 - 145 <br /> Commend: Reporting limit increased due to limited sample volume. <br /> OF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Enlcch Analytical Labs,Inc.(CA FLAP 82346) <br /> Patti Sandrock,QA/QC Manager Environmental Analysis Since 1983 <br />