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9 0 <br /> Entech ,analytical Labs, Inca <br /> 3334 Victor Court o Santa Clara, CA 95054 a (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Boa 802 Date Received: 3/13/2003 <br /> Benicia,CA 94510 Project Name: PG&E <br /> Project Number: 03400 00 <br /> .Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-018 Client Sample ID: B15-9 <br /> Sample Time: 2:45 PM Sample Dale: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag D6 PQL DLR Units Extraction Analysis QC Dutch ID M1iclhod <br /> Date Date <br /> Naphthalene ND 5 0.33 1.65 mglKg 3/13/2003 3/14/2003 BS5208B EPA 9270C <br /> 2-muthyhtuphdmhme 2.8 5 0.33 1.65 mg/KS 3/13/2003 3/14/2003 BS5208B EPA 9270C <br /> 2-Chloron tphtholene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Acenaphthylene ND 5 0.33 1.65 mg/Kg 3/132003 3/14/2003 BS52088 EPA 8270C <br /> Acenaphthene ND 5 0.33 1.65 mg/Kg 3/13/20D3 3/142003 BS52088 EPA 8270C <br /> Fiuorenc ND 5 0.33 1.65 mg/Kg 3/13/2003 3/142003 DS5208B EPA 8270C '.. <br /> Phenanthrene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Anthmcene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> nuoranthene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Pyrene ND 5 0.33 1.65 mg/Kg 3/1312003 3/14/2003 BS5208B EPA 8270C <br /> Bcnzo(a)muhmcenc ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Chrysene ND 5 0.66 3.3 mg/Kg 3/132003 3/14/2003 BS52088 EPA 8270C <br /> Bcnzu(b)iluommlicnc ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 827oC <br /> Ben to(k)(luommhenc ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Benzo(a)pyrene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/)42003 BS520811 EPA 8270C j <br /> Indcno(1,2,3-cd)pyrcne ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 DS520813 EPA 8270C <br /> Dibenz(a,h):mIlm cene ND 5 0.33 1.65 mg/Kg 3/132003 3/14/2003 SS5208B EPA 8270C '.. <br /> Benzo(gh,i)perylene ND 5 0.33 1.65 mg/Kg 3/13/2003 3/14/2003 BS5208B EPA 8270C <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 2-Plucrobiphenyl 57.4 30 - 115 <br /> Nitrobenzene-d5 45.9 23 - 120 <br /> p-Terphenyl-d14 94.2 18 - 137 <br /> Comment: Sample diluted due to the nature of the sample matrix. <br /> DF=Dilution Factor ND=Not Delceted DLR-Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Labs,Inc.(CA FLAP#2346) <br /> ,!�;,7 d � <br /> `�P'atti Sand ck,QA/QC Manager Environmental Analysis Since 1983 <br />