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r _ <br /> .... 'N,` ..y ,. ....._ .. _ ._..:_r ..., ,...._ ., ... _._ _-`-.... -.x,•: is-_ ,;c <br /> mss., ✓'. ... .. ,..:r ,rte., r..,. .. .. .. - -..., ._ r._.._....... ........:.- _.. -, _ _a-,J� ._n <br /> n 1 <br /> ✓' -. f ._ ✓ ..- .. .r, 1. ... _ .. .. .1.--v. ". ..-•: .:/ 1' r- __F- <br /> b <br /> i <br /> .ex <br /> PrIlk L n C <br /> _,•,, <br /> d dstel <br /> L-%boca <br /> a )n. s <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgt. Co. Group Number: 873149 <br /> Reported: 12/04/03 at 10:13 AM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL Units %REC %REC Limits RPD RPD Max <br /> Batch number: 033050016A Sample number(s) : 4155450-4155452 <br /> Total TPH N.D. 4.0 mg/kg 87 84 77-126 3 20 <br /> C10-C36 N.D. 4.0 mg/kg <br /> Batch number: 03306SLA026 Sample number(s) : 4155450-4155452 <br /> Naphthalene N.D. 1. ug/kg 62 56-130 <br /> Acenaphthylene N.D. 0.3 ug/kg 54* 58-119 <br /> Acenaphthene N.D. 0.3 ug/kg 59* 61-120 <br /> Fluorene N.D. 0.3 ug/kg 61* 66-125 <br /> Phenanthrene N.D. 0.3 ug/kg 57* 66-117 <br /> Anthracene N.D. 0.3 ug/kg 52* 64-116 <br /> Fluoranthene N.D. 0.7 ug/kg 54* 68-123 <br /> Pyrene N.D. 0.3 ug/kg 63 63-134 <br /> Benzo(a)anthracene N.D. 0.3 ug/kg 58* 69-119 <br /> Chrysene N.D. 0.3 ug/kg 61* 69-120 <br /> Benzo,(b)fluoranthene N.D. 0.3 ug/kg 63* 69-127 <br /> Benzo(k)fluoranthene N.D. 0.3 ug/kg 62* 72-119 <br /> Benzo(a)pyrene N.D. 0.3 ug/kg 59* 68-112 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.3 ug/kg 79 66-130 <br /> Dibenz(a,h)anthracene N.D. 0.3 ug/kg 72 62-131 <br /> Benzo(g,h,i)perylene N.D. 0.3 ug/kg 78 65-129 <br /> Batch number: 03307A34A Sample number(s) : 4155450-4155452 <br /> Benzene N.D. 0.005 mg/kg 105 86-113 <br /> Toluene N.D. 0.005 mg/kg 102 88-113 <br /> Ethylbenzene N.D. 0.005 mg/kg 102 89-112 <br /> Total Xylenes N.D. 0.02 mg/kg 101 90-112 <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 03306SLA026 Sample number(s) : 4155450-4155452 <br /> Naphthalene 58 60 33-140 3 30 <br /> Acenaphthylene 52* 54 53-123 3 30 <br /> Acenaphthene 58 59 29-139 3 30 <br /> Fluorene 61 63 26-153 4 30 <br /> Phenanthrene 57 58 56-123 2 30 <br /> Anthracene 53* 54* 55-129 2 30 <br /> Fluoranthene 64 66 16-175 4 30 <br /> Pyrene 59 59 4-190 1 30 <br /> Benzo(a)anthracene 58 58 50-140 1 30 <br /> Chrysene 60 60 36-144 1 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> (2) The background result was more than four times the spike added. <br /> r t ; <br /> ir <br />