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Geo,tnalytical Laboratories,-tnc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax (209)572-0916 <br /> Report# R026-06 CERTIFICATE OF ANALYSIS Date: 2/02/05 <br /> Date Rec'd: 1/26/05 <br /> Thorpe Oil Date Started: 1/31/05 <br /> PO Box 357 Project: 216 N.California St Stockton, CA Date Completed:1/31/05 <br /> Lodi CA 95241 Date Sampled: 1/26/05 <br /> PO# Time: 10:0 am <br /> Sample ID: EX-1 at 17' Sampler : R.Chrun(Geo) <br /> Lab ID: 8200113 <br /> Method RL Analyte Results Units <br /> 8260B 25 Benzene ND µg/Kg <br /> 25 Toluene ND <br /> 25 Ethyl Benzene ND <br /> 25 Total Xylenes ND <br /> 50 Methyl tert-butyl ether(MTBE) ND <br /> 200 Ethanol ND <br /> 1000 tert-Butanol ND <br /> 50 di-Isopropyl ether(D1PE) ND <br /> 50 Ethyl tert-butyl ether(ETBE) ND <br /> 50 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery OC Limit% <br /> *Surrogate criteria not met due to high level of 1,2-Dichloroethane-d4 100 107 107.0 66-133 <br /> non-target analyte concentration. 2-Bromo-l-chloropropane 100 110 110.0 63-139 <br /> Elevated detection limits due to high level of non target <br /> analyte Concentration. 4-Bromofluorobenzene 100 *157 157.0 64-136 <br /> Mari D'On�/,- Donna Keller <br /> Chemist Certification # 2585 Laboratory Director <br />