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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No.: H4122010 Date: 12129/2004 Page: 5 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8280FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-3R Lab Samp ID: 7660-4W <br /> Descr/Location: MW-3R Rec'd Date: 12120/20n4 <br /> Sample Date: 12/16/2004 Prep Date: 12/23/2004 <br /> Sample Time: 1120 Analysis Date: 12123/2004 <br /> Matrix: Water QC Batch: VMS-D234 <br /> Basis: Not Filtered Notes: ' <br /> Analyte Det Limit Rep limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.289 0.5 MRL a2 UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) M084 0.5 MRL ND UG/L 1 <br /> tort-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UG/L 1 <br /> DI-isopropyl ether(DIPE) 0.155 0.5 MRL ND UG/L 1 <br /> tort-Butyl alcohol (TBA) 8.79 20. MRL 22 UGIL 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL 26 UG/L 1 <br /> 12-Dibromoethane 0.092 0.5 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 63-132 SLSA 94.9% 1 <br /> 1,2-Dtchioroethane-d4 59-135 SLSA 91.0% 1 <br /> Approved by: Date: z <br />