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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3121802 Date: 12/29/2003 Page: 9 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-8S tab Samp ID: 6447-7W <br /> Descr/Location: MW-8S Recd Date: 12/1812003 <br /> Sample Date: 12/17/2003 Prep Date: 12/22/2003 <br /> Sample Time: 1400 Analysis Date: 12/22/2003 <br /> Matrix: Water QC Batch: VWMS-D223 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.289 0.5 MRL ND UG/L 1 <br /> Ethyl tent-butyl ether(ETBE) 0.084 0.5 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0.155 0.5 MRL 1.3 UG/L 1 <br /> tert-Butyl alcohol (TBA) 8.79 20. MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL Cl 71. UG/L 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 133% 1 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 105% 1 <br /> Cl: See narrative <br /> i <br /> Approved by:_ Date: 2-1016-V <br />