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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3092618 Date: 1 010 7/2 0 0 3 Page: 5 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-5 Lab Samp ID: 8164-4W <br /> Descr/Location: MW-5 Rec'd Date: 09/29/2003 <br /> Sample Date: 09/25/2003 Prep Date: 10/04/2003 <br /> Sample Time: 1230 Analysis Date: 10/04/2003 <br /> Matrix: Water QC Batch: VWMS-0043 <br /> Basis: Not Filtered Notes: BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.578 1. MRL ND UG/L 2 <br /> Ethyl tert-butyl ether(ETRE) 0.168 1. MRI, NO UG/L 2 <br /> tert-Amyl methyl ether(TAME) 0.134 1. MRL ND UG/L 2 <br /> Di-isopropyl ether(DIPS) 0.310 1. MRL ND UG/L 2 <br /> tert-Butyl alcohol (TBA) 17.6 40. MRL ND UG/L 2 <br /> 1,2-Dichloroethane 0.162 1. MRL 53 UG/L 2 <br /> 1,2-Dibromoethane 0.184 1. MRL NO UG/L 2 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SI_SA 111% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 101% 1 <br /> BH: Reporting limits raised due to high level of non-target analytes <br /> Approved by:. �.,_. Date: 16171za. .,,, <br />