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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3062702 Date: 07/10/2003 Page: 5 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 2ND QTR Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2R Lab Samp ID: 5858-4W <br /> Descr/Location: MW-2R Rec'd Date: 06/27/2003 <br /> Sample Date: 06/25/2003 Prep Date: 07/02/2003 <br /> Sample Time: 1200 Analysis Date: 07/02/2003 <br /> Matrix: Water QC Batch: VWMS-7023 <br /> Basis: Not Filtered Notes: OF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) Z89 5. MRL NO UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0.42 5. MRL NO UG/L 10 <br /> tert-Amyl methyl ether(TAME) 0.67 5. MRL NO UG/L 10 <br /> Dkisopropyl ether(DIPS) 1.55 5. MRL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 87.9 200. MRL ND UG/L 10 <br /> 1,2-Dichloroethane 0.81 5. MRL ND UG/L 10 <br /> 1,2-Dibromoethane 0.92 5. MRL ND UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76•129 SLSA 101% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 90.0% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> Approved by: 'Tt N 6 Date: <br />