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' Alpha Analytical, Inc. 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 Date: Work Order: 03-Jan-07 OC Summary Report 06120852 Sample Matrix Spike Type: MS Test Code: EPA Method SW60201 SW6020A File ID: 121306.BI009MSL.D1 Batch ID: 16366 Analysis Date: 12/14/200611 :13 Sample ID: 06120852-10AMS Units : mg/Kg Run ID: ICPIMS_061214B Prep Date: 12/13/2006 Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual Beryllium (Be) 20.9 1 25 0 83 66 137 Sodium (Na) 5350 100 5000 454.5 98 66 137 Magnesium (Mg) 29100 100 5000 18790 207 66 137 M3 Potassium (K) 5980 100 5000 2673 66 66 137 Calcium (Ca) 22900 100 5000 6435 329 66 137 M3 Vanadium (V) 83.6 1 25 79.98 14 66 137 M3 Chromium (Cr) 93.6 1 25 89.7 16 66 137 M3 Manganese (Mn) 1140 1 250 578.4 223 66 137 M3 Iron (Fe) 34900 500 5000 33740 22 66 137 M3 Cobalt (Co) 42. 1 1 25 16.46 103 66 137 Nickel (Ni) 149 2 25 127.8 84 66 137 Copper (Cu) 55.5 2 25 36.13 77 66 137 Zinc (Zn) 79.3 20 25 67.78 46 66 137 M3 Arsenic (As) 30.6 1 25 8.401 89 66 137 Selenium (Se) 21 .2 1 25 0 85 66 137 Molybdenum (Mo) 23.1 1 25 0 92 66 137 Silver (Ag) 23.3 1 25 0 93 66 137 Cadmium (Cd) 23.9 1 25 0 95 66 137 Antimony (Sb) 21 .6 1 25 0 86 66 137 Barium (Be) 411 1 250 185 90 66 137 Mercury (Hq) 0.554 0.2 0.5 0 111 48 144 Thallium (TI) 24.3 1 25 0 97 66 137 Lead (Pb) 30.9 1 25 6.921 96 66 137 Sample Matrix Spike Duplicate Type: MSD Test Code: EPA Method SW6020I SW6020A File ID: 121306.B1010MSD.D\ Batch ID: 16366 Analysis Date: 12/14/2006 11 :18 Sample ID: 06120852-10AMSD Units : mg/Kg Run ID: ICPIMS_061214B Prep Date: 12/13/2006 Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual Beryllium (Be) 21 .3 1 25 0 85 66 137 20.86 2.0(22) Sodium (Na) 5960 100 5000 454.5 110 66 137 5352 10.7(22) Magnesium (Mg) 28800 100 5000 18790 200 66 137 29130 1 .2(22) M3 Potassium (K) 8940 100 5000 2673 125 66 137 5984 39.6(22) R5 Calcium (Ca) 18700 100 5000 6435 246 66 137 22900 20.0(22) M3 Vanadium (V) 107 1 25 79.98 108 66 137 83.59 24.7(22) R58 Chromium (Cr) 119 1 25 89.7 119 66 137 93.62 . 24.2(22) R58 Manganese (Mn) 685 1 250 578.4 43 66 137 1137 49.6(22) M3 R58 Iron (Fe) 38100 500 5000 33740 87 66 137 34850 8.9(22) Cobalt (Co) 41 .1 1 25 16.46 99 66 137 42.1 2.3(22) Nickel (Ni) 154 2 25 127.8 104 66 137 148.8 3.4(22) Copper (Cu) 58.3 2 25 36.13 88 66 137 55.5 4.8(22) Zinc (Zn) 85.7 20 25 67.78 72 66 137 79.31 7.7(22) Arsenic (As) 29.8 1 25 8.401 86 66 137 30.61 2.7(22) Selenium (Se) 22.2 1 25 0 89 66 137 21 .24 4.2(22) Molybdenum (Mo) 22.8 1 25 0 91 66 137 23.12 1 .3(22) Silver (Ag) 23.8 1 25 0 95 66 137 23.32 2.0(22) Cadmium (Cd) 24 1 25 0 96 66 137 23.85 0.4(22) Antimony (Sb) 21 .6 1 25 0 86 66 137 21 .58 0.0(22) Barium (Be) 469 1 250 185 114 66 137 411 13.2(22) Mercury (Hq) 0.597 0.2 0.5 0 119 48 144 0.5539 7.5(22) Thallium (TI) 25.3 1 25 0 101 66 137 24.34 4.0(22) Lead (Pb) 31 .9 1 25 6.921 99.8 66 137 30.85 3.2(22)