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Alpha Analytical, Inc. 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431 -5778 (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 Date: Work Order: 03-Jars-07 - OC Summary Rewrt 06120852 Sample Matrix Spike Type: MS Test Code: EPA Method SW6020 File ID: 121306.B1034MS.D1 Batch ID: 16341 Analysis Date: 12113/2006. 15:21 Sample ID: 06120852.09AMS Units : mg/L Run ID: ICP/MS_061213B Prep Date: 12/1112006 Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Llmit) Qual Beryllium (Be) 0.262 0.004 0.25 0 105 _ 75 126 Sodium (Na) 285 0.5 50 237.9 95 75 126 Magnesium (Mg) 204 0.5 50 148.8 109 75 126 Aluminum (Al) 55. 1 0.2 50 0 110 75 126 Potassium (K) 54 0.5 50 0.7741 107 75 126 Calcium (Ca) 77.6 0.5 50 24.08 107 75 126 Vanadium (V) 0.281 0.003 0.25 0 112 75 126 Chromium (Cr) 0.278 0.005 0.25 0 111 75 126 Manganese (Mn) 4.21 0.005. 2.5 1 .568 106 75 126 Iron (Fe) 53.5 0.3 50 0 107 75 126 Cobalt (Co) 0.271 0.005 0.25 0 106 75 126 Nickel (Ni) 0.264 0.01 0.25 0 105 75 126 Copper (Cu) 0.264 0.01 0.25 0 106 75 126 Zinc (Zn) 0.254 0. 1 0.25 0 102 75 126 Arsenic (As) 0.276 0.005 0.25 0.01793 103 75 126 Selenium (Se) 0.253 0.005 0.25 0 101 75 126 Molybdenum (Mo) 0.26 0.005 0.25 0.01056 99.9 75 126 Silver (Ag) 0.248 0.005 0.25 0 99 75 126 Cadmium (Cd) 0.254 0.005 0.25 0 102 75 126 Antimony (Sb) 0.26 0.005 0.25 0 104 75 126 Barium (Be) 3.11 0.005 2.5 0.3953 108 75 126 Mercury (Hg) 0.00501 0.001 0.005 0 100 75 126 Thallium (TI) 0.245 0.002 0.25 0.008952 95 75 126 Lead (Pb) 0.264 0.005 0.25 0.005906 103 75 126 Sample Matrix Spike Duplicate Type: MSD Test Code: EPA Method SW6020 File ID: 121306.B%035MSD.D\ Batch ID: 16341 Analysis Date: 12/13/2006 15:26 Sample ID: 06120852.09AMSD Units : mg1L Run ID: ICP/MS061213B Prep Date: 12/11/2006 Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRetVal %RPD(Limit) Qual Beryllium (Be) 0.28 0.004 0.25 0 112 75 126 0.2619 6.5(10) Sodium (Na) 304 0.5 50 237.9 133 75 126 285.2 6.5(10) M3 Magnesium (Mg) 216 0.5 50 148.8 135 75 126 203.5 6.1 (10) M3 Aluminum (AI) 60 0.2 50 0 120 75 126 55.11 8.5(10) Potassium (K) 57.6 0.5 50 0.7741 114 75 126 54.03 6.5(10) Calcium (Ca) 85.8 0.5 50 24.08 124 75 126 77.56 10.1 (10) R58 Vanadium (V) 0.303 0.003 0.25 0 121 75 126 0.2808 7.6(10) Chromium (Cr) 0.302 0.005 0.25 0 121 75 126 0.278 8.3(10) Manganese (Mn) - 4.52 0.005 2.5 1 .568 118 75 126 4.213 6.9(10) Iron (Fe) 57.9 0.3 50 0 116 75 126 53.54 7.8(10) Cobalt (Co) 0.291 0.005 0.25 0 116 75 126 0.2711 7.1 (10) Nickel (Ni) 0.287 0.01 0.25 0 115 75 126 0.2637 8.3(10) Copper (Cu) 0.283 0.01 0.25 0 113 75 126 0.2644 6.7(10) Zinc (Zn) 0.271 0. 1 0.25 0 108 75 126 0.2541 6.5(10) Arsenic (As) 0.294 0.005 0.25 0.01793 110 75 126 0.2756 6.4(10) Selenium (Se) 0.266 0.005 0.25 0 107 75 126 0.2526 5.3(10) Molybdenum (Mo) 0.29 0.005 0.25 0.01056 112 75 126 0.2603 10.8(10) R5 Silver (Aq) 0.266 0.005 0.25 0 106 75 126 0.2479 7. 1(10) Cadmium (Cd) 0.276 0.005 0.25 0 110 75 126 0.254 8.3(10) Antimony (Sb) 0.28 0.005 0.25 0 112 75 126 0.2604 7.2(10) ! Barium (Ba) 3.37 0.005 2.5 0.3953 119 75 126 3.105 8.0(10) Mercury (Hg) 0.00543 0.001 0.005 0 109 75 126 0.005007 8.0(19) Thallium (TI) 0.271 0.002 0.25 0.008952 105 75 128 0.2454 9.8(10) Lead (Pb) 0.283 0.005 0.25 0.005906 111 75 126 0.2639 6.8(10)