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QA/QC Report <br /> Method Blank Summary <br /> Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2061306 Date 06/24/2002 Page 34 <br /> QC Batch WMS21598 Analysis Volatile Organic Compounds by GC/MS <br /> Matrix Water Method SW8260B <br /> Lab Samp ID WM821598 Prep Meth SW5030B <br /> Analysis Date 06/18/2002 Prep Date 06/18/2002 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Bromobenzene 02 5 PQL ND UG/L 1 <br /> n-Butylbenzene 02 5 PQL ND UGIL 1 <br /> sec-Butylbenzene 02 5 PQL NO UGIL 1 <br /> tent-Butylbenzene 07 5 PQL ND UGIL 1 <br /> 2-Chlorotoluene 01 5 PQL NO UGIL 1 <br /> 4-Chlorotoluene 01 5 PQL ND UGIL 1 <br /> cis-1,2-DEchloroethene 03 5 PQL NO UGIL 1 <br /> 1,3-Dichloropropane 03 5 PQL ND UG/L 1 <br /> 2,2-Dichloropropane 02 5 PQL ND UGIL 1 <br /> 1,1-Dichloropropene 02 5 PQL NO UGIL 1 <br /> 4-Isopropyltoluene 01 5 PQL NO UGIL 1 <br /> Methyl-tert-butyl ether(MTBE) 03 5 PQL ND UG/L 1 <br /> n-Propylbenzene 02 5 PQL ND UGIL 1 <br /> 1,2,3-Tnchlorobenzene 05 5 PQL ND UGIL 1 <br /> 1,2,4-Tnmethylbenzene 03 5 PQL ND UGIL 1 <br /> 1,3,5-Trimethylbenzene 02 5 PQL ND UGIL 1 <br /> Cyclohexanone 20 20 PQL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 05 5 PQL NO UGIL 9 <br /> Ethyl tert-butyl ether(ETRE) 05 5 PQL NO UGIL 1 <br /> Hexane 5 20 PQL NO UGIL 1 <br /> tert-Amyl methyl ether(TAME) 03 5 PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 11 20 PQL ND UGIL 1 <br /> Tetrahydrofuran 20 20 PQL NO UGIL 1 <br /> Xylenes 1 06 5 PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 943% 1 <br /> Toluene-d8 65-135 SMSA 105% 1 <br /> Dibromofluoromethane 57-139 SMSA 108% 1 <br /> • <br />