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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Ph (209)384-2930 <br /> Fax <br /> Certificate#2480 <br /> Fax (209)384-1507 <br /> Foothill Engineering Client Project ID Vogue Cleaners Method EPA 5030/8015M,8020 <br /> 8442 Story Ridge Way Reference Number 8664 Instrument ID Var-GCi <br /> Antelope,CA 95843 Sample Description Water Extracted 1 D-24-05 <br /> Attn Mike Vlach Analyst Jim Phillips Analyzed 10-24-05 <br /> Reported 11-03-05 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Gasoline MTBE Benzene Toluene Ethyl Benzene Total Xylenes <br /> Spike Concentration 110 2 16 1 34 758 182 888 <br /> Units ug/L ug/L ug/L ug/L ug1L ug/L <br /> LCS Batch# VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 <br /> LCS%Recovery 105% 902% 103% 960% 103% 100% <br /> Surrogate Recovery 98 9°A 957% 957% 957% 957% 957% <br /> . Control Limas 70-130% 70-130% 70-130% 70-130% 70-130% 70-130% <br /> MS/MSD Batch# VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 VW-0245bhp2 <br /> Spike Concentration 110 2 16 1 34 758 182 888 <br /> MS%Recovery 971% 950% 105% 982% 103% 102% <br /> Surrogate Recovery 105% 103% 103% 103% 103% 103% <br /> MSD%Recovery 101% 149% 107% 101% 105% 105% <br /> Surrogate Recovery 106% 103% 103°x6 103% 103% 103% <br /> Relative%Difference 337% 440% 218% 2,42% 2 41% 278% <br /> Method Blank ND ND ND ND ND ND <br /> Surrogate Recovery 100% 102% 102% 102% 102% 102% <br /> The LCS(Laboratory Check Sample)is a control sample of known,interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents,preparation and analytical methods employed for the samples The LCS%recovery is used for validation <br /> of sample batch results Due to matrix effects,the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results <br /> APPROVED BY <br /> James C Phifit /Laboratory Director or <br /> Clan J Cone/ eboratory Manager <br />