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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone (209)384-2930 <br /> Fax (249)384-1507 <br /> Foothill Engineering Client Project ID Vogue Cleaners Method EPA 5030/8264 <br /> 8442 Story Ridge Way Reference Number 8664 Instrument ID HP Series II <br /> Antelope,CA 95843 Matrix Soil Prepared 14-2405 <br /> Attn Mike Vlach Analyst S Foster Analyzed 10-24-05 <br /> Reported 11-03-05 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID VSMS-0245 <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kg mg/Kgmg/Kg mg/Kg %R <br /> COMPOUNDS <br /> t-Bu I Alcohol(t-BA) 0 800 ND 300 906% 563-153 <br /> Methyl t-butyl l ether MTBE 0 010 ND 0100 988% <br /> 604-137 <br /> Diiso ro I ether DIPS 0 010 ND 010D 104% 700-130 <br /> Ethyl t-Butyl ether ETRE 0 010 ND 0 100 996% 700-130 <br /> t-Am I methyl ether AME 0 010 ND 0 100 816% 700-130 <br /> i 2-Dichloroethane(1,2-DCA) 0 010 ND 0 100 112% 636-138 <br /> Ethylene dibromide EDB 0 010 ND 0 100 992% 667-129 <br /> 1,1-Dichloroethane 1 1 DCE 0 010 ND 0 100 964% 545-154 <br /> Benzene 0 010 ND 0 100 111% 70 0-130 <br />. Tnchloroethene CE 0 010 ND 0 100 103% 700-130 <br /> Toluene 0 010 ND 0 100 108% 700-130 <br /> Chtorobenzene 0 010 ND 0 100 103% 700-130 <br /> D bromofluoromethane 0 010 1 106% 0 400 1131 667-132 <br /> 1,2-Dichloroethane-d4 0 010 108% 0 400 993% 592-135 <br /> Toluene-d8 0 010 102% 0 4629-132 <br /> 4-Bromofluorobenzene 4 010 401% 0 400 102% 697-131 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> mg/Kg %R %R <br /> COMPOUNDS <br /> t-Bu I Alcohol t-BA <br /> 300 767% 641% 553-153 179% <br /> Methvi t-butyl ether MTBE 0100 684% 568% 604-137 185% <br /> Diiso ro I ether RIPE 0 100 740% 572% 700-130 256% <br /> Ethyl t-Butyl ether ETBE 0 100 688% 524% 700-130 271% <br /> t-Am l methyl ether TAME 0 100 568% 376% --- 700-130 407% <br /> 1 2-Dichloroethane 1,2-DCA 0 100 712% 596% 636-138 177% <br /> Ethylene dibromide EDB 0 100 748% 536% 66 7- 129 330% <br /> 1 1-Dichloroethane 1 1 DCE 0 100 620% 440% 545-154 340% <br /> Benzene 0 100 760% 588% 700-130 255% <br /> Trichloroethene(TCE) 0 100 756% 576% 700-130 270% <br /> Toluene 0 100 764% 592% 700-130 254% <br /> Chlorobenzene 0 100 772% 560% 700-130 318% <br /> Surro ate <br /> Dibromofluoromethane 0 400 813% 69 5% 667-132 156% <br /> 1,2-Dichloroethane-d4 0 400 738% 609% 592-136 192% <br /> Toluene-d8 0 400 760% 657% .629-132 145% <br /> 4-Bromofluorobenzene 0 400 1 782% 702% 697-131 108% <br /> APPROVED BY Je <br /> Jame hr lips/CpWory Director or <br /> Clan J Cons/Lebo tory Manager <br />