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i <br /> analysis for no longer than the maximum allowable holding time Details on the procedures for <br /> collection and handling of samples used on this project can be found in this section and in the <br /> attached DQI tables <br /> Soil and Water Sample Labeling and Preservation <br /> Label information includes a unique sample identification number, lob identification number, date, <br /> and time After labeling, all soil and water samples are placed in a Ziploc® type bag and placed in an <br /> ice chest cooled to approximately 4°C Chemical preservation is controlled by the required analysis <br /> and is noted on the chain-of-custody form Trip blanks supplied by the laboratory accompany the <br /> groundwater sample containers and groundwater samples <br /> Upon recovery, the sample container is sealed to minimize the potential volatilization and cross- <br /> contamination prior to chemical analysis Soil sampling tubes are typically closed at each end with <br /> TeflonT"" sheeting and plastic caps The sample is then placed in a Ziploc® type bag and sealed <br /> The sample is labeled and refrigerated at approximately 4° Celsius for delivery, under strict chain-of- <br /> custody, to the analytical laboratory <br /> Chain of Custody <br /> The chain-of-custody form is used to record possession of the sample from the time of collection to <br /> its arrival at the laboratory When samples are shipped, the person in custody of them relinquishes <br /> the samples by signing the chain-of-custody form and noting the time The sample-control officer at <br /> the laboratory verifies sample integrity and conforms that the samples are collected in the proper <br /> containers, preserved correctly, and contain adequate volumes for analysis These conditions are <br /> noted on a Laboratory Sample Receipt Checklist (see attached) which will be included in the <br /> laboratory report <br /> If these conditions are met, each sample is assigned a unique log number for identification <br /> throughout analysis and reporting The log number is recorded on the chain-of-custody form and in <br /> the legally-required log book maintained by the laboratory The sample description, date received, <br /> client's name, and other relevant information is recorded <br /> Analytical Methods <br /> Soil and groundwater samples collected during exploratory sire investigation activities and <br /> development and sampling of monitoring wells, will be analyzed under a standard 10-day turnaround <br /> time Samples are analyzed using analytical methods outlined in EPA Manual SW 846 and approved <br /> by the California Regional Water Quality Control Board- Central Valley Region in the Leaking <br /> Underground Fuel Tanks (LUFT) manual and appendices <br /> Samples collected during the investigation of petroleum hydrocarbon impacted sites are typically <br /> analyzed for total petroleum hydrocarbons ([C2-C12 range] TPHG, BTEX, and oxygenates using EPA <br /> Method 82608 and total petroleum hydrocarbons ((Cla-C24])TPHd using EPA Method 8015 <br /> The attached DQI tables present the state-certified laboratory's calibration and quality assurance <br /> procedures for the above mentioned analytical methods Internal laboratory quality assurance <br /> checks will be the responsibility of the contract laboratories Data and reports submitted by field <br /> personnel and the contract laboratory will be reviewed and maintained in the project files <br /> Data Review and Verification <br />