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(p S4 <br /> 110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> Inc.4 McCampbell Analytical, Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell corn E mail main@mecampbell corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 03/28/05 <br /> Date Received 03/29/05 <br /> 837 Shaw Road <br /> Client Contact Tim Cuellar Date Extracted 04/01/05-04/05/05 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 04/01/05-04/05/05 <br /> Oxygenates and BTEX by GCIMS* <br /> Extraction Method SW5030D Analytical Method SW8260B Work Order 0503501 <br /> Lab ID 0503501-OOIB 0503501-002B 0503501-003B 10503501-004B <br /> Client ID MW-1 MW-2 MW-4 MW-5 Reporting Limit for <br /> ' DF=1 <br /> Matrix W W W W <br /> E <br /> DF 1 5 ; 1 1 S W <br /> I I <br /> Compound Concentration ug/kg ug/L <br /> ten-Amyl methyl ether(TAME) ND ND<2 5 ND ND NA 0 5 <br /> Benzene ND ND<2 5 ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND 43 ND ND NA 50 <br /> Dusopropyl ether(DIPE) ND ND<2 5 ND ND NA 0 5 <br /> Ethanol ND ND<250 ND ND NA 50 <br /> Ethylbenzene ND ND<2 5 ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND<2 5 ND ND NA 0 5 <br /> Methanol ND ND<2500 ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND 130 067 ND NA 0 5 <br /> Toluene ND ND<2 5 ND ND NA 05 <br /> Xylenes ND ND<2 5 ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SSI 99 100 101 IN <br /> %SS2 104 104 103 97 <br /> %SS3 114 115 114 110 <br /> Comments <br /> *water and vapor samples are reported in lig/L,soil/sludge/solid samples to mg/kg,productloil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L wipe samples in pg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> I <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--1 vol %sediment,j)sample diluted due to high <br /> organic content/matrix interference,k)reporting limit near but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> Ireporting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />