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u in <br /> 110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798 1622 <br /> Z4 L Website www mccampbell corn irmail mamQemccarnpbell corn <br /> • Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 03/28/05 <br /> 837 Shaw Road <br /> Date Received 03/29/05 <br /> Client Contact Tim Cuellar Date Extracted 04101105-04105105 <br /> Stockton, CA 95215 <br /> Client P O Date An 04/01/05-04105105 <br /> Oxygenates and BTEX by GC/MS* <br /> Extrachon Method SW5030B Analytical Method SW8260B Work Order 0503501 <br /> Lab ID 0503501-021B 0503501-022B 0503501-023B 0503501-024B <br /> Client ID MW-13C MW-13D ! MW-14 T MW-15 Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF I 1 1 5 S W <br /> Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND<2 5 NA 05 <br /> Benzene ND ND ND ND<2 5 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND 38 NA 50 <br /> Dnsopropyl ether(DIPE) ND ND ND ND<2 5 NA 0 5 <br /> Ethanol ND ND ND ND<250 NA 50 <br /> • Cthylbenzenc ND ND ND ND<2 5 NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND ND<2 5 NA 0 5 <br /> Methanol ND ND ND ND<2500 NA 500 <br /> Methyl-t-butyl ether(MTBE) ND ND 58 110 NA 05 <br /> Toluene ND ND ND ND<2 5 NA 0 5 <br /> Xylenes ND ND ND ND<2 5 NA 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 103 105 116 101 <br /> %SS2 104 103 94 103 <br /> %SS3 123 120 114 117 <br /> Comments 777—:�:j —I I <br /> *water and vapor samples are reported toµg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in pg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen product is present,t)liquid sample that contains greater than—1 vol %sediment,})sample diluted due to high <br /> organic content/matrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative <br /> DHS Certification No 1644 Angela Rydellus,Lab Manager <br />