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tr Slq <br /> 11 o 2nd Avenue South,ND7 Pacheco,CA 94553 5560 <br /> McCaIIlpbell Analytical, Inc. Telephone 925-798 1620 Fax 925 798-1622 <br /> Website www mccampbell com E-tnmil main@mccampbel]com <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 03/29/05 <br /> Date Received 03/30/05 <br /> 837 Shaw Road <br /> Client Contact Tim Cuellar Date Extracted 04104/05-04105/05 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 04104105-04105105 <br /> Oxygenates and BTEX by GCIMS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0503532 <br /> Lab ID 0503532-OOIB 0503532-002B 0503532-003B 0503532-004B <br /> Client 1D MW-11A MW-11BMW-1lC MW-i 1D Reporting Limit for <br /> DF=1 <br /> Matrix W W W W <br /> DF i 1 <br /> 1 1 S W <br /> � E <br /> Compound Concentration uglkg 1L�L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> Benzene ND ND ND ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 5 0 <br /> Dusopropyl ether(D1PE) ND ND ND ND NA 0 5 <br /> Ethanol ND ND ND ND NA 50 <br /> Ethylbenzene ND ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 0 5 <br /> Methanol ND ND ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) 5 4 18 ND ND NA 05 <br /> Toluene ND ND ND ND NA 0 5 <br /> Xylenes ND ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %S81 100 102 111 99 <br /> %SS2 104 91 96 92 <br /> %SS3 125 99 118 100 <br /> Comments <br /> water and vapor samples are reported inµg/L,soillsludgelsolid samples in mglkg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples inµg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than—I vol %sediment,j)sample diluted due to high <br /> organic content/matrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting limit raised due to insufficient sample amount,n results are reported on a dry wei ht basis, see attached narrative <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />