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� 11� <br /> Inc110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, I • Telephone 925 ell 1620 Fax 925 7mcca 2 <br /> F4 Website www nx:campbel]corn E mai1 mam©mccanrp6ell cam <br /> QC SUMMARY REPORT FOR SW8021BI8015Cm <br /> W O Sample Matrix Water <br /> QC Matrix Water WorkOrder 0503532 <br /> EPA Method SW8021B18015Cm Extraction 5W5030B <br /> 8atch1D 15652 Spiked Sample ID 0503531-002A <br /> Sample Spiked MS' MSD' MS-MSD' LCS LCSD LCS-LCSD Acceptance Criteria (%) <br /> Analyte <br /> Ng/L uglL % Rec % Rec %RPD %Rec % Rec % RPD MS!MSD LCS 1 LCSD <br /> TPH(btex) <br /> £ ND 60 92 3 94 5 230 974 998 237 10- 130 1 70- 130 <br /> MTBE ND l0 102 100 149 98 3 91 2 749 70- 130 70- 130 <br /> Benzene ND 10 107 109 1 28 108 101 705 70-130 , 70- 130 <br /> Toluene ND 10 100 102 225 103 102 1 37 70- 130 70- 130 <br /> Ethylbenzene ND 10 101 103 2 77 107 Inc 208 70 130 i i 70- 130 <br /> Xylenes ND 30 86 1 903 491 95 1 95 3 1 0 350 70-130 I 70- 130 <br /> %SS 110 10 117 115 1 184 112 ` 106 542 70- 130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 15552 SUMMARY <br /> Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> Sample ID Date Sampled Date Extracted <br /> 0503532 OOlA 3!29105 1D 29 AM 4102105 2 59 AM 4102105 2 59 AM=0503532-002A3/29/059105 10 44 AM 4102105 3 32 AM 4102105 3 32 AM <br /> 0503532-003A 3129105 11 06AM 4102105 4 04 AM 4102105 4 04 AM9105 1 1 23 AM 4102105 4 37 AM 4102105 4 37 AM <br /> 0503532-005A 3129105 8 48 AM 4102105 6 51 PM 4102105 6 51 PM129105 9 01 AM 41021055 42 AM 4102105 S 42 AM <br /> 0503532-007A 3!29105 9 18 AM 4102105 6 14 AM4102105 6 14 AM129105 9 37 AM 4102105 6 47 AM 4102105 6 47 AM <br /> i <br /> MS=Mainz Spike MSD=Matrix Spike Duplicate LCS=Lahoratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=loo'(MS-Sample)!(Amount Spiked) RPD=100'(MS- MSD)/((MS+MSD)/2) <br /> reasons a)the <br /> AND conSaDinsps gn4hcanl concenirauons of analytmaye relativ.to the ll outside of laboratory <br /> moutnt spiked orb)the spiked sample's matrix interferes with ghe spike recovery sample is inhomogenous <br /> £TPH(btex)=sum of STEX areas from the FID <br /> • #cluttered chromatogram sample peak coelutes with surrogate peak <br /> NIA=not applicable or not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=anal a concentration in sample exceeds s ike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to hi h matrix or analyte concent <br /> DHS Certification No 1644 QA/QC Officer <br />