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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccambbell co m E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Chent Project ID Flag City Chevron Date Sampled 12/14/00 <br /> 4005 North Wilson Way Date Received 12/15/00 <br />' Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 12/15-12/17/00 <br /> Client P O Date Analyzed 12/15-12/17/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 56046 56047 56048 56049 <br /> CSAI/ CSA2/ MW8A/ Reporting Limit <br /> Client ID 121400 121400 SP1/12]400 121400 <br /> Matrix W W S. W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> tert-Butanol ND ND ND ND 25 50 <br /> Methanol ND ND -- ND 1000 200 <br /> Ethanol ND ND - ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 105 106 100 106 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />