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I <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell coin E-mail main@mccampbell cam <br /> IAdvanced GeoEnvironmental Client Project ID Flag City Chevron Date Sampled 12/14/00 <br /> 4005 North Wilson Way Date Received 12/15/00 <br /> IStockton,CA 95205 Client Contact Tim Cuellar Date Extracted 12/15-12/17/00 <br /> I Client P O Date Analyzed 12/15-12/17100 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 56058 56059 56060 56061 <br /> MW 10D/ MWl OE/ MWI I A/ MW I I B/ Reporting Limit <br /> Client ID 121400 121400 121400 121400 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND<2 5 ND<5 0 50 10 <br /> IEthyl tent-Butyl Ether(ETBE) ND ND ND<2 5 ND<5 0 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND 140 260 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<2 5 ND<5 0 50 t 0 <br /> tert-Butanol ND NDND<l 2 5 ND<25 25 50 <br /> IMethanol ND ND ND<500 ND<1000 1000 200 <br /> IEthanol ND ND ND<t25 ND<250 250 50 <br /> Surrogate Recoveries(%) <br /> IDibromofluoromethane 71 105 105 104 104 <br /> Comments <br /> *water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> i <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />