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McCampbell Analytical, Inc. 1102 Avenue25 7 #D7,Pacheco CA 981622560 Tel hone 925 798 1620 Fax 925-798 1G22 - — - - - - - Website www mccampbell com E-mail main@mccampbell cora -- Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 (0 837 Shaw Road Date Received 01/23/04 Client Contact Tim Cuellar Date Extracted 01/23/04 Stockton,CA 95215 Client P O Date Analyzed 01/24/04-01/28/04 Serra-Volatile Organics by GC/MS(Basic Target List)* Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 Lab ID 0401260-004D - Client ID - P42-40to44 Matrix Water Compound Concentration* DF i a,m s Compound Concentration * DF aLamg Acenaphthene ND 10 10 Acenaphthylene ND lo 10 Anthracene ND 10 10 Benzidine NO 10 50 Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 10 10 Benzo(b)fluoranthene ND 1 0 10 Benzo k fluoranthene ND 1 0 10 Benzo(g li,i)perylene ND 1 0 10 Benzo(a)pyrene ND 10 10 Ben ]Alcohol ND ix )Methane ND 1 0 10 Bis 2-chloroeth 1)Ether ND 1 0 10 Bis 2-chloroiso ra i Ether ND 1 0 10 Bis 2-eth ]hex 1)Phthalate ND 1 0 10 4-13romophenyl Phenyl Ether ND 1 0 10 Bu ]ben 1 Phthalate ND 1 0 10 4-Chloroanitme ND 1 0 20 4-Chloro-3-meth i henol ND 1 0 10 2-Chlorona hthalene ND 1 0 10 2-Chlorophenol ND 1 0 10 4-Chloro hen 1 Phenyl Ether ND 10 10 Chrysene ND 10 10 Dibenzo(a,h)anthracene ND 10 10 Dibenzofuian ND 1 0 10 Di-n-but 1 Phthalate ND 10 10 12-Dtchlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 1,4-Dichlorobenzene I ND 10 10 3,3-Dichlorobenzidtne ND 10 20 2,4-Dichloro henol ND l 0 10 Diethyl Phthalate ND 10 10 2 4-Dimethylphenol ND 1 0 10 Dimethyl Phthalate ND 10 10 4,6-Dimtro-2-meth l henol ND 10 50 2,4-Dmltro heno] ND 10 50 2 4-Dmitrotoluene ND 1 1 0 10 2 6-Dinitrotoluene ND 10 10 Dt-n-octyl Phthalate ND 10 10 1 2-Di hen ]h drazme ND 10 10 Fluoranthene ND 10 10 Fluorene ND 10 10 Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 1 10 Hexachloroc clopentadiene ND 10 50 Hexachlometbane ND 1 0 10 Indeno 1,2,3-cd)pyrene ND 10 10 Iso horone ND lo 1 10 2-Meth lna hthalene ND 1 0 10 2-Meth 1 heno/(o-Cresol) ND 10 10 3 Wor 4-Meth 1 henol(m, -Cresol) ND 1 0 10 Naphthalene ND 10 10 2-Nitroanrline ND 10 T 50 3-Nitroaniline ND 10 50 4-Nitroantlme ND 10 1 50 1 Nitrobenzene ND 10 50 2-Nitro heno) ND 10 50 1 4-Nitrophenol ND 10 10 N-Nitrosodi hen lamme ND 10 10 N-Nitrosodi-n-propylamine ND 1 0 10 Pentachlorophenol ND l 0 50 Phenanthrene ND 10 10 Phenol ND 10 10 Pyrene ND 10 10 1,2,4-Trichlorobenzene ND 1 0 10 2,4,5-Trichlorophenol ND 10 10 2,4,6-Trichlorophenol ND 1 0 10 Surrogate Recoveries(%) %SSI 999 %SS2 103 %SS3 91 8 %SS4 863 %SS5 88 1 { %SS6 83 3 Comments t *water samples and all TCLP 8c SPLP extracts are reported inµg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/oil/non- aqueous liquid samples in mg/L ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis #)surrogate diluted out of range,&)low or no surrogate due to matrix interference h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,a)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable concentration but under the RL for this compound DHS Certification No 1644Angela RydeIius, Lab Manager J