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110 2nd Avenue South #D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell com Email inain@rnccarrTbell com-- — — <br /> Advanced GcoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01122/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analyhcal Method. SW8270D Work Order 0401260 <br /> Lab ID 0401260-023A <br /> Client ID - P42-50' <br /> Matrix Soil <br /> Compound Concentration* DF x t`pO,,,`w,a Compound Concentration* DF Reporting <br /> s <br /> Acenaphthene ND 1 0 0 33 1 Acenaphthylene ND l 0 1 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 1 6 Benzoic Acid ND 1 0 1 6 <br /> Benzo a anthracene ND 1 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo k fluoranthene ND 1 0 033 Benzo g,h i erylene ND 10 033 <br /> Benzo(a)pyrene ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis(2-chloroetbox )Methane ND 1 0 033 Bis(2-chloroethl)Ether ND 1 0 1 033 <br /> Bis 2-chlormso ro 1)Ether ND 1 0 0 33-1 Bis 2-eth ]hex 1 Adt ate ND 1 0 033 <br /> Bis 2�th ]hex ! Phthalate ND 1 0 0 33 4-13romo hen 1 Phenyl Ether ND 10 033 <br /> Butylbenal Phthalate ND to 0 33 4-Chloroaniline ND 10 066 <br /> Nitrobenzene ND 1 0 16 4-Chloro-3-meth ]phenol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol ND 10 033 <br /> 4-Chloro hen I Phcn l Ether ND 1 0 033 Chrysene ND l 0 033 <br /> Dibenzo a,h anthracene ND 10 033 Dibenzofuran ND 1 0 033 <br /> Di-n-bu l Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> • l,3-Dichlorobenzene ND 11 0 033 1,4-DiOlorobenzene ND 10 033 <br /> 3 3-Dichlorobenzidine ND 1 0 066 2,4-Dichloro henol ND 10 033 <br /> Diethyl Phthalate ND 1 0 033 2 4-Dimethylphenol ND 10 033 <br /> Dimethyl Phthalate I ND 1 0 033 4,6-13mitro-2-meth l henol ND 1 1 0 16 <br /> 2 4-Dinitrohenol ND 10 16 2,4-Dimtrotoluene ND 10 033 <br /> 2,6-Dimtrotoluene ND 1 0 1 033 Di-n-oct I Phthalate ND 10 033 <br /> 1,2-Di hen Ili drazine ND 1 0 033 Flueranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clo entadiene ND 10 16 <br /> Hexachlomethane ND 1 1 0 033 Indeno 1,2,3-cd)pyrene ND 10 033 <br /> Iso horone ND 1 0 033 2-Meth Ina hthalene ND l 0 0 33 <br /> 2-Meth l henol(o-Cresol) ND 1 0 033 3 Wor 4-Methylphenol m, -Cresol ND 1 0 033 <br /> Naphthalene ND 1 0 0 33 2-Nitroamlme ND 1 0 1 6 <br /> 3-Nitroanilme ND 10 16 4-Nitroaniline ND 10 16 <br /> 2-Nitrophenol ND 1 0 1 6 4-Nitrophenol ND 1 0 033 <br /> N-Nitrosodi hen lamme ND 1 0 033 N-Nitrosodi-n7propylamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND TO 033 <br /> Phenol ND 1 0 033 Pyrene ND 1 0 0--43 <br /> 1,2,4-Tnchlorobenzene ND 1 0 033 2,4,5-Trichloro henol ND 10 1 033 <br /> 2,4,6-Trichlorophenol ND _10 0-3 3 <br /> Surrogate Recoverles(%) <br /> %SS l 95 5 %SS2 870 <br /> %SS3 894 %SS4 86 1 <br /> %SS5 796 %SS6 862 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in Ag/L,soiUsludge/solid samples to mg/kg,wipe samples inµg/wipe,productloil/non- <br /> aqueous liquid samples in mglL <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,I)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 VAngela Rydelius, Lab Manager <br />