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� l� 110 2nd Avenue South #D7,Pacheco,CA 94553-5560 <br /> FMcCampbell Analytical, Inc Telephone 925-798 1620 Fax 925 798-1622 <br /> h //www ince bell coin E-mail ruain(a)inceampbell corn <br /> S QC SUMMARY REPORT FOR SW8270D <br /> Matrix S Work0rder 0401260 <br /> EPA Method SW8270D Extraction SW3550C BatchlD 10069 Spiked Sample ID 0401260-013A <br /> Sample Spiked MS* MSD' MS-MSD' LCS LCSD ILCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec %Rec %RPD %Rec % Rec %RPD Low High <br /> Acenaphthene ND 2 75 8 797 507 82 5 824 0 109 30 130 <br /> 4-Chloro-3-methylphenol ND 4 81 847 451 805 798 0 898 30 130 <br /> 2-Chlorophenol ND 4 867 895 320 87 987 194 30 130 <br /> 1,4-Dichlorobenzene ND 2 81 1 845 414 876 88 0 444 30 130 <br /> 2,4-Dmltrotoluene ND 2 71 8 763 602 799 779 247 30 130 <br /> 4-Nitrophenol ND 4 77 797 349 752 723 394 30 130 <br /> N-Nitrosodi-n-propylarnine ND 2 81 82 l 19 819 806 1 56 30 130 <br /> Pentachlorophenol ND 4 782 765 2 19 786 782 0 587 30 130 <br /> Phenol ND 4 774 799 3 11 798 80 1 0 450 30 130 <br /> Pyrene ND 2 81 2 861 580 982 887 0 475 30 130 <br /> 1,2,4-Tnehlorobenzene ND 2 113 911 552 174 967 0 742 30 130 <br /> %SS l 946 200 81 4 861 560 85 1 84 1 36 30 130 <br /> %SS2 928 200 947 82 320 879 877 0 280 30 130 <br /> %SS3 86 1 200 867 924 641 98 8 978 104 30 130 <br /> %SS4 869 200 84 1 889 5 54 91 2 91 5 0 257 30 130 <br /> %SS5 823 200 814 857 5 14 876 854 264 30 130 <br /> %SS6 874 200 78 7 849 l 767 83 183 6 0 574 30 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> MS=Matnx Spike MSD=Matrix Spike Duplicate,LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent <br /> Deviation <br /> %Recovery=100*(MS-Sample)/(Amount Spiked),RPD=100*(MS- MSD)!((MS+MSD)/2) <br /> *MS and J or MSD spike recovenes may not be near 100%or the RPDs near 0%if a)the sample is inhomogenous AND contains significant concentrations of <br /> analyte relative to the amount spiked or b)if that specific sample matrix interferes with spike recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or <br /> analyte content <br /> &=low or no surrogate due to matnx interference <br /> Laboratory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels / <br /> DHS Certification No 1644 T QA/QC Officer <br />