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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> 14 McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-798 1622 <br /> Website www mccampbell Mtn E mail main@=canipbell cam <br /> . Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> CIient Contact Tun Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/23/04-01/26/04 <br /> Oxygenated Volatile Organics-+-EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method Sw8260B Work Order 0401260 - <br /> Lab ID 0401260-005C i 0401260-006C 0401260-007C 0401260-008C <br /> i <br /> Client ID P40A-14to 19 P40A-47to51 P39-15to20 P39-36to41 Reporting Limit for <br /> DF=1 <br /> Matrix W W W i W <br /> DF ---- - 5--- - -- ----�- I 1 i 50� s W <br /> Compound <br /> Concentration u> g 1ig/L <br /> tert-Amyl methyl ether(TAME) ND<2 5 ND ND ND<25 50 05 - <br /> t-Butyl alcohol(TBA) ND<25 ND ND ND<250 25 5 0 <br /> 1,2-Dibromoethane(EDB) ND<2 5 ND ND ND<25 50 05 <br /> 1 2-Dichloroethane(1,2-DCA) ND<2 5 ND ND ND<25 50 05 <br /> Ditsopropyl ether(D1PE) ND<2 5 ND ND ND<25 50 05 <br /> Ethyl tert-butyl ether(ETBB) ND<2 5 ND ND ND<25 50 05 <br /> Methyl-t-butvl ether(MTBE) 120 15 ND 570 5 0 05 <br /> Surrogate Recoveries{%) <br /> %SS 976 999 977 930 <br /> Comments t <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in gg/kg, wipe samples in}Ag/wipe <br /> product/oil/non-aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> t <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 r\I, A 7 Angela Rydehus, Lab Manager <br />