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w, NELAP Certification 01103CA FLAP Certification 1664 <br /> Caltest <br /> ENVIRONMENTAL ANALYSES <br /> LAB ORDER No 0120219 <br /> LABORATORY CONTROL SAMPLE ANALYTICAL RESULTS Page 10 of 15 <br /> SPIKE SPIKE\DUP SPK\DUP ACCEPTANCE REL% <br /> ANALYTE AMOUNT RESULT XREC %REC \RPD DIFF ANALYZED NOTES <br /> QC BATCH R020148PAH (continued) <br /> POLYNUCLEAR AROMATIC HYDROCARBONS (PAH) 12 11 02 <br /> (continued) <br /> Fluorene 4 00 1 80\ 45\ 28-74\25 <br /> Pyrene 4 00 2 77\ 69\ 40-93\25 <br /> Surrogate p-Terphenyl 4 00 3 00\ 75\ 59-114\ <br /> QC BATCH S020107BNA <br /> SEMIVOLATILE ORGANIC COMPOUNDS 12 16 02 <br /> 2 4-Dinitrotoluene 50 0 43 9\ 88\ 30-130\22 <br /> N-Nitrosodi-n-propylamine 50 0 33 1\ 66\ 30-130\21 <br /> 4-Chloro-3-methylphenol 100 56 8\ 57\ 10-130\35 <br /> 2-Chlorophenol 100 53 0\ 53\ 28-117\25 <br /> 4-Nitrophenol 100 47 7\ 48\ 20-120\24 <br /> Pentachlorophenol 100 97 3\ 97\ 20-140\20 <br /> henol 100 24 5\ 24\ 20-120\56 <br /> urrogate Nitrobenzene-d5 50 0 28 8\ 58\ 20-120\ <br /> urrogate 2-Fluorobiphenyl 50 0 27 9\ 56\ 10-120\ <br /> Surrogate Terphenyl-d14 50 0 44 5\ 89\ 30-130\ <br /> Surrogate 2-Fluorophenol 100 41 7\ 42\ 20-120\ <br /> Surrogate Phenol-d6 100 30 1\ 30\ 10-120\ <br /> Surrogate 2 4 6-Tribromophenol 100 82 2\ 82\ 30-140\ <br /> QC BATCH T0203520CP <br /> CHLORINATED PESTICIDES & PCBS 12 12 02 1 <br /> Aldrin 0 200 0 126\ 63\ 30-130\25 <br /> gamma-BHC (Lindane) 0 200 0 162\ 81\ 59-93\20 <br /> p p' -DDT 0 200 0 180\ 90\ 30-127\14 <br /> Dieldrin 0 200 0 173\ 87\ 63-107\17 <br /> Endrin 0 200 0 171\ 86\ 44-117\22 <br /> Heptachlor 0 200 0 145\ 72\ 28-104\17 <br /> Surrogate TCMX 0 200 0 122\ 61\ 14-78\ <br /> Surrogate Decachlorobiphenyl 0 200 0 170\ 85\ 38-115\ <br /> 1) This sample was analyzed following Florisil column cleanup (EPA Method 3620B) <br /> 1885 North Kelly Road • Napa, California 94558 <br /> (707)258-4000 • Fax (707)226-1001 • e-mail caltest@caltestlab com - <br />