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, N <br /> BSKANALYTICAL <br /> LABORATORIES <br /> Chari a <br /> y Heang Certificate of Analysis <br /> Caltest Analytical Laboratory ELAP Certificate#1180 <br /> 1885 N Kelly Road Report issue Date 01/22/2003 <br /> Napa, CA 94558 <br /> BSK Submission#: 2002120386 <br /> BSK Sample ID#• 272992 <br /> Protect lD 0120220 Project Desc <br /> Submission Comments <br /> Sample Type Liquid Date Sampled 12/05/2002 <br /> Sample Descnptton Flag City Chevron Eff Time Sampled 1438 <br /> Sample Comments Date Received 12/06/2002 <br /> Inorganics Prep Analysis <br /> Analyte Method Result Units MDL ML Dilution DLR Date Date <br /> Chromium-Hexavalent(Cr+6) EPA 218 6 0.30 pg/L 016 02 1 02 12/06/2002 12/06/2002 <br /> Nitrate(NO3-N) EPA 300 0 11 mg/L 001 02 2 04 12/09/2002 12/09/2002 H <br /> Organics <br /> Prep Analysis <br /> Analyte Method Result Units MDL ML Dilution DLR Date Date <br /> Dibromochlo opropane EPA 504 1 ND pg1L 0 007 001 1 001 12/09/2002 12/12/2002 <br /> Ethylenedibromide EPA 504 1 ND pg/L 0 004 002 1 002 12/09/2002 12/12/2002 <br /> i <br /> 2,4,5-TP(Siivex) EPA 515 3 ND pg/L 042 10 1 1 12/11/2002 12/12/2002 <br /> 2,4-D EPA 515 3 ND pg/L 53 10 1 10 12/11/2002 12/12/2002 <br /> Sentazon(Basagran) EPA 515 3 ND 1ig/L 084 20 1 2 12/11/2002 12/12/2002 <br /> Dalapon EPA 515 3 ND gg/L 16 10 1 10 12/11/2002 12/12/2002 <br /> Dinoseb(DNBP) EPA 515 3 ND pg/L 049 20 1 2 12/11/2002 12/12/2002 <br /> Pentachlorophenol(PCP) EPA 515 3 ND pg/L 002 02 1 02 1211112002 12/12/2002 <br /> Picloram EPA 515 3 ND pg/L 027 10 1 1 12!11/2002 12/12/2002 <br /> Alachlor(Alanex) EPA 525 2 ND pg/L 03 10 1 1 12/16/2002 12/18/2002 <br /> Atrazine(AAtrex) EPA 525 2 ND pg/L 08 10 1 1 12!16/2002 12/18/2002 <br /> bts(2-ethyihexyl)adipate EPA 525 2 ND pg/L 051 30 1 3 12/16/2002 12/I812002 <br /> Diazinon EPA 525 2 PID pg/L 010 025 1 025 12/16/2002 12/18/2002 <br /> Molitiate(Qrdram) EPA 525 2 ND gg/L 028 20 1 2 12/16/2002 12/18/2002 <br /> Simazine(Princep) EPA 525 2 ND pg/L 038 10 1 1 12/16/2002 12/18/2002 <br /> Thiobencarb(Bolero) EPA 525 2 ND gg/L 045 10 1 1 12/16/2002 12/18/2002 <br /> CarboSuan EPA 531 1 ND 4g/L 13 50 1 50 12/22/2002 12/22/2002 <br /> Oxamyl EPA 531 1 PID pg/L 26 200 1 20 12/22/2002 12/22/2002 <br /> DNQ=Detected,not quantified The trace values between the MDL and DLR are of an unknown data quality Baseline noise, <br /> calibration curve extrapolation below the lowest calibrator,method blank detections,and integration artifacts can all produce apparent <br /> DNQ values,which contribute to the un-reliability of these values <br /> mg/L Milligrams/Liter(ppm) MDL Method Detection Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Prelimmary result <br /> pg/L Micrograms/Literb PQL x Dilution <br /> � ) ND None Detected above MDI S Suspect resulk See Cover Letter for comments <br /> pg/Kg Acrograms/Kilogram(ppb) E Analysis performed by External Iaboratory <br /> °/uRec Percent Recovered(surrogates) ML Practical Quantitation Limit See External Laboratory Report attachments <br /> DNQ Detected,Not Quantified DNQ Trace Result( MDL,<DLR Trace results are only qualitative values(estimates) <br /> Report Authentication Code 1®1111111NI111011®O111i1Q101[Mimi III]IV111111111111M11 Page 1 of <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />