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110 tad Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798 1622 <br /> h //www mrcanipbcfl corn E-mail bell cum <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/27/03 <br /> 837 Shaw Road Date Received 01/28/03 <br /> Client Contact Tim Cuellar Date Extracted 01/29/03-01/30/03 <br /> Stockton,CA 95215 <br /> rc—lient—P 0 Date Analyzed 01/29/03-01/30/03 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0301345 <br /> Lab ID 0301345-OOIC 0301345-002C f <br /> Client ID Influent Effluent <br /> Reporting Limit for <br /> Matrix W ---W 3--- – ---- DE=i <br /> DF 1 1 ; S W <br /> Compound Concentration ug/kg µg/L <br /> Diisopropyl ether(DIPE) ND ND NA 05 <br /> Ethyl tent-butyl ether(ETRE) ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) 21 ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND NA 50 <br /> Methanol ND ND NA 500 <br /> Ethanol ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND NA 05 <br /> iSurrogate Recoveries(%) <br /> %SS 104 103 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in lig/L,soillsludgelsolid samples in gg/kg, wipe samples in Fig/wipe, <br /> product/oil/non-aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />