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110 2nd Avenue South ##D7 Pacheco CA 94553-5560 <br /> LA <br /> 1VIcCampbell Analytical Inc Telephone 925-790 1620 Fax 925-798-1622 <br /> 6ttp llwww mccampbell cam E-mail main®mccampbell corn <br /> . Advanced GeoEnvlronmental,Inc Client Project ID Flag City Chevron Date Sampled 09/05/02 <br />' 837 Shaw Road Date Received 09/06/02 <br /> CIient Contact Tim Cuellar Date Extracted 09/06/02 <br /> Stockton,CA 95215 <br />' <br /> Lc=hent <br /> Date Analyzed 09/06/02 <br /> Lead by Graphite Furnace Atomic Absorption* <br /> xtrackon method E200 7 Analytical methods E200 9 Work Order 0209081 <br />' Lab ID Client ID Matrix Extraction Lead DF %SS <br /> 0209081-028C INFLUENT W TTLC ND I NIA <br /> 1 <br /> Reporting Limit for DF=1, W TTLC 0 005 mg/L <br /> ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> *water samples are reported in mg/L,soil/sludge/solid/product samples in mg/kg,wipes in ug/wipe and all TCLP I STLC I DISTLC I SPLP extracts in <br /> mg/L <br /> ND means not detected above the reporting limit,N/A means not applicable to this sample or instrument <br /> Analytical Methods EPA 61110020117 for all elements except 200 9(water-Sb,As,Pb,Se,Tl),245 1 (Hg),7010(sludge/soil/solyd/ml/product/wipes- <br /> IAs,Se,Tl),7471B(Hg) <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the extraction fluid <br /> DISTLC results are not applicable to STLC regulatory limits <br /> i)liquid sample that contains greater than—2 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> • significantly effect reported metal concentrations,z)reporting limit raised due to matrix interference <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />