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i BSKANALYTICAL LABORATORIES i QC Summary Report 10/01/2002 1111111 Ilill 11(11 IllllIIIII Illll Illll IIIIIIIIIIIIIII/III/III BSK Submission 2002090292 Client Caltest Analytical Laboratory Date Subrmtted 09/06/2002 Project ID C090158 Project Desc BSK StarLlms Run # 43156 (1111111111119111111111111Ell 1111 Instrument ID GC9 Analyst Initials. JENNIFERD Method Number 504 1 Surrogate Results Analyte QC Type Surr Result UCL LCL Date — ----- ------ - ----� �.----- -------------- — ———— Bromoform RBLK N/A 111 6 %Rec 140 60 09/14/02 Acceptable BSK StarLims Run # 43298 11111 11111111111111/111111111111 Instrument 19 SVGCMS2 Analyst Initials DANB y Method Number 525 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Cone Cone UCL LCL Date Alachlor(Alanex) LCS NIA 483 µg/L 96 5 ND 130 70 09/16/02 Acceptable Benzo(a)pyrene LCS N/A 3 21 µg/L 107 3 ND 130 70 09/16/02 Acceptable bis(2-ethylhexyl)adipate LCS N/A 504 ltg/L. 100 5 ND 130 70 09/16/02 Acceptable bis(2-ethylhexyl)phthalate LCS N/A 547 µg/L 109 5 ND 130 70 09/16/02 Acceptable ButachlOr LCS N/A 309 µg/L 103 3 ND 130 70 09/16/02 Acceptable • Metolachlor LCS N/A 476 µglL 95 5 ND 130 70 09/16/02 Acceptable Molmate(Ordram) LCS N/A 453 µg/L 90 5 ND 130 70 09/16/02 Acceptable Prometryn(Caparol) LCS N/A 589 ug/L 117 5 ND 130 70 09/16/02 Acceptable Propachlor LCS N/A 4 4 µg/L 88 5 ND 130 70 09/16/02 Acceptable Thiobencarb(Bolero) LCS N/A 499 pg/L 99 5 ND 130 70 09/16/02 Acceptable Alachlor(Alanex) LCSD N/A 465 µg/L 93 3 8 5 ND 130 70 09/16/02 Acceptable Benzo(a)pyrene LCSD N/A 349 µg/L 116 83 3 ND 130 70 09/16/02 Acceptable bts(2-ethylhexyl)adipate LCSD N/A 5 51 µg/L 110 9 5 ND 130 70 09/16/02 Acceptable bis(2-ethylhexyl)phthalate LCSD N/A 5 4 µg/L 108 1 2 5 ND 130 70 09/16/02 Acceptable Butachlor LCSD N/A 3 1 µg/1- 103 032 3 ND 130 70 09/16/02 Acceptable Metolachlor LCSD N/A 471 µg/L 94 1 5 ND 130 70 09/16/02 Acceptable Mohnate(Ordram) LCSD N/A 428 µg/L 85 57 5 ND 130 70 09/16/02 Acceptable Prometryn(Caparol) LCSD N/A 566 µg/L 113 4 5 ND 130 70 09/16/02 Acceptable Propachlor LCSD N/A 424 µg/L 84 38 5 ND 130 70 09/16/02 Acceptable Thiobencarb(Bolero) LCSD N/A 471 µg/1- 94 58 5 ND 130 70 09/16/02 Acceptable ------------ --------- ---------------------- — Alachlor(Alanex) RBLK NIA 0 µg11- <1 1 N/A 09/16/02 Acceptable Atrazine(AAtrex) RBLK N/A 0 µg/L <1 1 NIA 09/16/02 Acceptable Benzo(a)pyrene RBLK N/A 0 µg11- <O 1 01 NIA 09/16/02 Acceptable bis(2-ethylhexyl)adipate RBLK N/A 0 µg/L <3 3 N/A 09/16/02 Acceptable bis(2-ethylhexyl)phthalate RBLK N/A 0 141- <3 3 NIA 09/16/02 Acceptable Bromacil(Hyvar) RBLK N/A 0 µg/L <10 10 N/A 09/16/02 Acceptable Butachlor RBLK N/A 0 µg/L <039 0 38 N/A 09/16/02 Acceptable Diazinon RBLK N/A 0 µg/1- <025 0 25 NIA 09/16/02 Acceptable Dtmethoate(Cygon) RBLK N/A 0 µg/L <10 10 N/A 09/16/02 Acceptable • Metolachlor RBLK N/A 0 µg/L <05 0 5 NIA 09/16/02 Acceptable %Rec Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 3 of 6 RPD Relative Percent Difference OOS-Htgh QC Result Above UCL UCL Upper Control Lirmt OOS-Low QC Result Below LCL LCL Lower Control Limit