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BSKANALYTICAL LABORATORIES QC Summary Report 10/01/2002 I Ilill!IIIII illll IIIII Illll Illll IIIA VIII IIlI!Illll llil III! BSK Submission 2002090292 Client Caltest Analytical Laboratory Date Submitted 09/06/2002 Project ID C090158 Project Desc BSK StarLtmS Run # 43604 1111111IM11HIM loll 11111 ME III] Instrument ID HPLCI Analyst Initials TIMC Method Number 531 1 Surrogate Results Analyte QC Type Surr Result UCL LCI., Date BDMC LCSD N/A 100 2 %Rec 82 120 80 09/21/02 Acceptable BDMC w ——— — MS — 243770 95 3 %Rec 77 120 80 09/21/02 Acceptable --- --- ___________ BDMC RBLK N/A — 82 %Rec ———— ——————— 120 80 09/21/02 Acceptable BSK StarLims Run # 43907 IMilo 1111111111111111MEIII Instrument ID HPLC1 Analyst Initials TIMC Method Number 547 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike ID Result Units or RPD RPD Conc Cone UCL LCL Date Glyphosate LCS N/A 196 Ag/L 98 200 ND 120 80 09/24/02 Acceptable Glyphosate LCSD N/A 181 µg/L 90 58 200 ND 120 80 09/24/02 Acceptable Glyphosate MS 243873 1713 n/L 85 200 ND 120 80 09/24/02 Acceptable . Glyphosate ————— — — — — —— —MSD 243873 177 8pg/L 883 8 200 ND 120 — 80 09/24/02— NIA 0 Pg/L <25 Acceptable Glyphosate RBLK T 25 N/A 09/24/02 Acceptable Surrogate Results Analyte QC Type Surr Result UCL LCL Date AMPA LCS N/A 91 0 %Rec 862 120 80 09/24/02 Acceptable AMPA LCSD N/A 93 0 %Rec 862 120 80 09/24/02 Acceptable AMPA MS 243873 99 2 %Rec 892 120 80 09/24/02 Acceptable AMPA — ————— MSD — 243873 —�89 5 %Rec 892 120 80 09/24/02 Acceptable --- — --- -- -------------------- ---------- AMPA RBLK N/A 86 2 %Rec 120 80 09/24/02 Acceptable Approved by %Rec Percent Recovered Parent Sample Sample used as background matrix for MS/MSD Page 6 of 6 RPD Relative Percent Difference OOS-High QC Result Above UCL UCL Upper Control Limit OOS-Low QC Result Below LCL LCL Lower Control Limit